C₃₃H₂₈O₇S₂⁽²⁾H₈⁽¹³⁾C

Base Information

Chemical Name:C₃₃H₂₈O₇S₂⁽²⁾H₈⁽¹³⁾C
CAS No.:1036431-45-4
Molecular Formula:C₃₄H₃₆O₇S₂
Molecular Weight:629.713
Hs Code.:

C<sub>33</sub>H<sub>28</sub>O<sub>7</sub>S<sub>2</sub><sup>(2)</sup>H<sub>8</sub><sup>(13)</sup>C

Synonyms:C₃₃H₂₈O₇S₂⁽²⁾H₈⁽¹³⁾C

Suppliers and Price of C₃₃H₂₈O₇S₂⁽²⁾H₈⁽¹³⁾C

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₂₈O₇S₂⁽²⁾H₈⁽¹³⁾C

Chemical Property:

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Technology Process of C₃₃H₂₈O₇S₂⁽²⁾H₈⁽¹³⁾C

There total 14 articles about C₃₃H₂₈O₇S₂⁽²⁾H₈⁽¹³⁾C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1036431-44-3
C₁₆⁽²⁾H₈H₁₀O₂S⁽¹³⁾C

: 1036431-45-4
C₃₃H₂₈O₇S₂⁽²⁾H₈⁽¹³⁾C

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methanethiolate / methanol; dimethylformamide

2: methanol; dimethylformamide

With sodium thiomethoxide; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/jlcr.1404

Reference yield:

: 1036431-42-1
C₁₄⁽²⁾H₉H₇O₂⁽¹³⁾C

: 1036431-45-4
C₃₃H₂₈O₇S₂⁽²⁾H₈⁽¹³⁾C

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / Et₃N / CH₂Cl₂

2: 71 percent / cesium carbonate / dimethylformamide

3: sodium methanethiolate / methanol; dimethylformamide

4: methanol; dimethylformamide

With caesium carbonate; triethylamine; sodium thiomethoxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/jlcr.1404

Reference yield:

: 1036431-36-3,350818-57-4
C₈⁽²⁾H₇H₃O

: 1036431-45-4
C₃₃H₂₈O₇S₂⁽²⁾H₈⁽¹³⁾C

Guidance literature:: Multi-step reaction with 12 steps

1: N-bromosuccinimide / CCl₄ / Irradiation

2: 79 percent / 18-crown-6 / acetonitrile / 4 h / Heating

3: 80 percent / Na; deuterium oxide / 3 h / Heating

4: 91 percent / deuterium bromide / 0.08 h / 150 °C / microwave irradiation

5: 91 percent / DIEA / acetonitrile / microwave irradiation

6: lithium aluminum deuteride / diethyl ether

7: deuterium oxide; deuterium chloride

8: 91 percent / EtOD; NaOD

9: 94 percent / Et₃N / CH₂Cl₂

10: 71 percent / cesium carbonate / dimethylformamide

11: sodium methanethiolate / methanol; dimethylformamide

12: methanol; dimethylformamide

With N-Bromosuccinimide; lithium aluminium deuteride; deuteriated sodium hydroxide; 18-crown-6 ether; ethyl [2]alcohol; water-d2; sodium; hydrogen chloride; deuterium bromide; caesium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium thiomethoxide; In methanol; tetrachloromethane; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/jlcr.1404