ethyl N-[(S)-N-benzyloxycarbonylpyrrolidine-2-ylmethanesulfonyl]glycinate

Base Information

Chemical Name:ethyl N-[(S)-N-benzyloxycarbonylpyrrolidine-2-ylmethanesulfonyl]glycinate
CAS No.:1454845-63-6
Molecular Formula:C₁₇H₂₄N₂O₆S
Molecular Weight:384.453
Hs Code.:

Synonyms:ethyl N-[(S)-N-benzyloxycarbonylpyrrolidine-2-ylmethanesulfonyl]glycinate

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Chemical Property of ethyl N-[(S)-N-benzyloxycarbonylpyrrolidine-2-ylmethanesulfonyl]glycinate

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Technology Process of ethyl N-[(S)-N-benzyloxycarbonylpyrrolidine-2-ylmethanesulfonyl]glycinate

There total 2 articles about ethyl N-[(S)-N-benzyloxycarbonylpyrrolidine-2-ylmethanesulfonyl]glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 623-33-6
glycine ethyl ester hydrochloride

: 212204-36-9
Cbz-Pro-ψ[CH2SO2]-Cl

: 1454845-63-6
ethyl N-[(S)-N-benzyloxycarbonylpyrrolidine-2-ylmethanesulfonyl]glycinate

Guidance literature:: With triethylamine; In dichloromethane; at 35 ℃; Cooling with ice;
DOI:10.1016/j.tet.2013.08.028

Reference yield:

: 101250-72-0
(S)-2-Acetylsulfanylmethyl-pyrrolidine-1-carboxylic acid benzyl ester

: 1454845-63-6
ethyl N-[(S)-N-benzyloxycarbonylpyrrolidine-2-ylmethanesulfonyl]glycinate

Guidance literature:: Multi-step reaction with 2 steps

1: N-chloro-succinimide; hydrogenchloride / water; acetonitrile / 10 - 20 °C

2: triethylamine / dichloromethane / 35 °C / Cooling with ice

With hydrogenchloride; N-chloro-succinimide; triethylamine; In dichloromethane; water; acetonitrile;
DOI:10.1016/j.tet.2013.08.028