Technology Process of C36H36N8OSSi
There total 5 articles about C36H36N8OSSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
4,7-bis[(trimethylsilyl)ethynyl]benzo[c][1,2,5]thiadiazole;
With
potassium hydroxide;
In
methanol; water;
at 20 ℃;
Inert atmosphere;
C23H24N6O;
With
copper(ll) sulfate pentahydrate; sodium L-ascorbate;
In
dichloromethane; water;
at 20 ℃;
for 12h;
DOI:10.1016/j.tetlet.2013.01.119
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium azide / N,N-dimethyl-formamide / 90 °C
2.1: piperidine / acetonitrile / Inert atmosphere; Reflux
3.1: potassium hydroxide / methanol; water / 20 °C / Inert atmosphere
3.2: 12 h / 20 °C
With
piperidine; sodium azide; potassium hydroxide;
In
methanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tetlet.2013.01.119
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine / dichloromethane
2.1: sodium azide / N,N-dimethyl-formamide / 90 °C
3.1: piperidine / acetonitrile / Inert atmosphere; Reflux
4.1: potassium hydroxide / methanol; water / 20 °C / Inert atmosphere
4.2: 12 h / 20 °C
With
piperidine; sodium azide; triethylamine; potassium hydroxide;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tetlet.2013.01.119
