Carbamic acid, (3-cyclopenten-1-ylmethyl)-, 1,1-dimethylethyl ester (9CI)

Base Information

Chemical Name:Carbamic acid, (3-cyclopenten-1-ylmethyl)-, 1,1-dimethylethyl ester (9CI)
CAS No.:207729-05-3
Molecular Formula:C₁₁H₁₉NO₂
Molecular Weight:197.277
Hs Code.:
Mol file:207729-05-3.mol

Synonyms:Carbamic acid, (3-cyclopenten-1-ylmethyl)-, 1,1-dimethylethyl ester (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, (3-cyclopenten-1-ylmethyl)-, 1,1-dimethylethyl ester (9CI)

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

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Technology Process of Carbamic acid, (3-cyclopenten-1-ylmethyl)-, 1,1-dimethylethyl ester (9CI)

There total 6 articles about Carbamic acid, (3-cyclopenten-1-ylmethyl)-, 1,1-dimethylethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 4492-42-6
(cyclopent-3-ene)methylamine

: 207729-05-3
tert-butyl cyclopent-3-enylmethylcarbamate

Guidance literature:: With triethylamine; In methanol; at 50 ℃; for 1h;
DOI:10.1016/S0040-4020(99)00596-7

Reference yield:

: 25125-21-7
4-(hydroxymethyl)cyclopentene

: 207729-05-3
tert-butyl cyclopent-3-enylmethylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 4-methyl-morpholine / tetrahydrofuran / 20 h / 20 °C

2.1: sodium azide / N,N-dimethyl-formamide / 20 h / 60 °C

3.1: water; triphenylphosphine / tetrahydrofuran / 4 h / 80 °C

3.2: 1.5 h / 4 - 20 °C

With 4-methyl-morpholine; sodium azide; water; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1364687-10-4
C₆H₉N₃

: 207729-05-3
tert-butyl cyclopent-3-enylmethylcarbamate

Guidance literature:: C₆H₉N₃; With water; triphenylphosphine; In tetrahydrofuran; at 80 ℃; for 4h;

di-tert-butyl dicarbonate; In tetrahydrofuran; water; at 4 - 20 ℃; for 1.5h;