Technology Process of C37H45NO8
There total 20 articles about C37H45NO8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C37H45NO7;
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; water;
In
tetrahydrofuran; tert-butyl alcohol;
at 10 ℃;
for 24h;
With
water; ammonium chloride;
In
tetrahydrofuran; tert-butyl alcohol;
DOI:10.1021/ol1027877
- Guidance literature:
-
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; water;
In
tetrahydrofuran; tert-butyl alcohol;
at 10 - 25 ℃;
for 48h;
DOI:10.1021/ol1027877
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium carbonate / dimethyl sulfoxide / 1.5 h / 55 °C
2.1: ammonium acetate; acetic acid / 6 h / 100 °C
3.1: lithium borohydride; chloro-trimethyl-silane / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere
4.1: tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
4.2: 8 h / 60 °C / Inert atmosphere
5.1: trichlorophosphate / 0.75 h / Cooling with ice
5.2: 0.25 h / 100 °C / Microwave irradiation; Sealed tube
5.3: Heating
6.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene; water / tetrahydrofuran; tert-butyl alcohol / 24 h / 10 °C
With
sodium chlorite; sodium dihydrogenphosphate; lithium borohydride; chloro-trimethyl-silane; 2-methyl-but-2-ene; ammonium acetate; water; potassium carbonate; acetic acid; trichlorophosphate;
In
tetrahydrofuran; dimethyl sulfoxide; tert-butyl alcohol;
5.2: Vilsmeier-Haack formylation / 6.1: Lindgren oxidation;
DOI:10.1021/ol1027877
