C₄₂H₆₈O₃SSi

Base Information

• Chemical Name: C₄₂H₆₈O₃SSi
• CAS No.: 1020736-10-0
• Molecular Formula: C₄₂H₆₈O₃SSi
• Molecular Weight: 681.152
• Mol file: 1020736-10-0.mol

Synonyms:C₄₂H₆₈O₃SSi

Chemical Property of C₄₂H₆₈O₃SSi

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₄₂H₆₈O₃SSi

There total 1 articles about C₄₂H₆₈O₃SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

C22H32O2S (1020736-08-6) + ((1S,3R)-3-((E)-5-bromo-3-methylpent-3-enyl)-2,2-dimethyl-4-methylenecyclohexyloxy)(tert-butyl)dimethylsilane (1020736-06-4) → C42H68O3SSi (1020736-10-0)

Guidance literature:

C₂₂H₃₂O₂S; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h; Inert atmosphere;

((1S,3R)-3-((E)-5-bromo-3-methylpent-3-enyl)-2,2-dimethyl-4-methylenecyclohexyloxy)(tert-butyl)dimethylsilane; In tetrahydrofuran; hexane; for 4h; Inert atmosphere;

DOI:10.1021/ol800326n

Reference yield: 83.0%

C42H68O3SSi (1020736-10-0) → C36H64OSi (1020736-20-2)

Guidance literature:

C₄₂H₆₈O₃SSi; With lithium; ethylamine; In tetrahydrofuran; at -78 ℃; for 0.5h;

With water; ammonium chloride; In tetrahydrofuran; methanol; for 0.166667h;

DOI:10.1021/ol800326n

upstream raw materials:

C₂₂H₃₂O₂S

((1S,3R)-3-((E)-5-bromo-3-methylpent-3-enyl)-2,2-dimethyl-4-methylenecyclohexyloxy)(tert-butyl)dimethylsilane

Downstream raw materials:

C₃₆H₆₄OSi