6-[3-chloro-2-(phenylsulfanyl)propylsulfanyl]-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one

Base Information

• Chemical Name: 6-[3-chloro-2-(phenylsulfanyl)propylsulfanyl]-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one
• CAS No.: 1221155-04-9
• Molecular Formula: C₂₀H₁₇ClN₄OS₂
• Molecular Weight: 428.966
• Mol file: 1221155-04-9.mol

Synonyms:6-[3-chloro-2-(phenylsulfanyl)propylsulfanyl]-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one

Chemical Property of 6-[3-chloro-2-(phenylsulfanyl)propylsulfanyl]-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of 6-[3-chloro-2-(phenylsulfanyl)propylsulfanyl]-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one

There total 1 articles about 6-[3-chloro-2-(phenylsulfanyl)propylsulfanyl]-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

6-allylsulfanyl-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one (850911-53-4) + benzenesulfenyl chloride (931-59-9) → 6-[3-chloro-2-(phenylsulfanyl)propylsulfanyl]-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one (1221155-04-9) + C20H17N4OS2(1+)*ClO4(1-)

Guidance literature:

With lithium perchlorate; In acetic acid; at 15 - 20 ℃;

DOI:10.1134/S1070428009120161

Reference yield: 85.0%

6-[3-chloro-2-(phenylsulfanyl)propylsulfanyl]-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one (1221155-04-9) → 1-phenyl-7-phenylsulfanyl-7,8-dihydro-6H-pyrazolo[3',4':4,5]pyrimido[2,1-b][1,3]thiazin-4(1H)-one (1221155-05-0)

Guidance literature:

With sodium acetate; In dimethyl sulfoxide; at 60 ℃; for 1h;

DOI:10.1134/S1070428009120161

upstream raw materials:

6-allylsulfanyl-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one

benzenesulfenyl chloride

Downstream raw materials:

1-phenyl-7-phenylsulfanyl-7,8-dihydro-6H-pyrazolo[3',4':4,5]pyrimido[2,1-b][1,3]thiazin-4(1H)-one