N-(E)-{3,3-bis[(benzyloxy)methyl]-6-(trimethylsilyl)hex-5-yn-1-ylidene}-1-phenylmethanamine

Base Information

• Chemical Name: N-(E)-{3,3-bis[(benzyloxy)methyl]-6-(trimethylsilyl)hex-5-yn-1-ylidene}-1-phenylmethanamine
• CAS No.: 745062-62-8
• Molecular Formula: C₃₂H₃₉NO₂Si
• Molecular Weight: 497.753

Synonyms:N-(E)-{3,3-bis[(benzyloxy)methyl]-6-(trimethylsilyl)hex-5-yn-1-ylidene}-1-phenylmethanamine

Chemical Property of N-(E)-{3,3-bis[(benzyloxy)methyl]-6-(trimethylsilyl)hex-5-yn-1-ylidene}-1-phenylmethanamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(E)-{3,3-bis[(benzyloxy)methyl]-6-(trimethylsilyl)hex-5-yn-1-ylidene}-1-phenylmethanamine

There total 1 articles about N-(E)-{3,3-bis[(benzyloxy)methyl]-6-(trimethylsilyl)hex-5-yn-1-ylidene}-1-phenylmethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

benzylamine (100-46-9) + 3,3-bis[(benzyloxy)methyl]-6-(trimethylsilyl)hex-5-ynal → N-(E)-{3,3-bis[(benzyloxy)methyl]-6-(trimethylsilyl)hex-5-yn-1-ylidene}-1-phenylmethanamine (745062-62-8)

Guidance literature:

With magnesium sulfate; In benzene; at 20 ℃;

DOI:10.1055/s-2004-822398

Reference yield: 91.0%

N-(E)-{3,3-bis[(benzyloxy)methyl]-6-(trimethylsilyl)hex-5-yn-1-ylidene}-1-phenylmethanamine (745062-62-8) → (E)-N-benzyl-4,4-bis[(benzyloxy)methyl]-2[(trimethylsilyl)methylene]cyclopentanamine

Guidance literature:

With dibutylbis(cyclopentadienyl)zirconium; In tetrahydrofuran; at 20 ℃; for 1.5h;

DOI:10.1055/s-2004-822398

Reference yield: 91.0%

acetyl chloride (75-36-5) + N-(E)-{3,3-bis[(benzyloxy)methyl]-6-(trimethylsilyl)hex-5-yn-1-ylidene}-1-phenylmethanamine (745062-62-8) → N-benzyl-N-{(2E)-4,4-bis[(benzyloxy)methyl]-2-[(trimethylsilyl)methylene]cyclopentyl}acetamide

Guidance literature:

N-(E)-{3,3-bis[(benzyloxy)methyl]-6-(trimethylsilyl)hex-5-yn-1-ylidene}-1-phenylmethanamine; With dibutylbis(cyclopentadienyl)zirconium; In tetrahydrofuran; at 20 ℃; for 1.5h;

acetyl chloride; In tetrahydrofuran; at -78 - 20 ℃; for 2h;

DOI:10.1055/s-2004-822398

upstream raw materials:

benzylamine

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 745062-62-8 N-(E)-{3,3-bis[(benzyloxy)methyl]-6-(trimethylsilyl)hex-5-yn-1-ylidene}-1-phenylmethanamine

Send

Send

Metric Ton KG G Pound L ML

Send

Send