N-(2-amino-5-methylbenzoyl)-8-amino-2-methyl-5,11-methano-5,6,11,12-tetrahydrodibenzo[b,f][1,5]diazocine

Base Information

Chemical Name:N-(2-amino-5-methylbenzoyl)-8-amino-2-methyl-5,11-methano-5,6,11,12-tetrahydrodibenzo[b,f][1,5]diazocine
CAS No.:334874-40-7
Molecular Formula:C₂₄H₂₄N₄O
Molecular Weight:384.481
Hs Code.:

Synonyms:N-(2-amino-5-methylbenzoyl)-8-amino-2-methyl-5,11-methano-5,6,11,12-tetrahydrodibenzo[b,f][1,5]diazocine

Suppliers and Price of N-(2-amino-5-methylbenzoyl)-8-amino-2-methyl-5,11-methano-5,6,11,12-tetrahydrodibenzo[b,f][1,5]diazocine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(2-amino-5-methylbenzoyl)-8-amino-2-methyl-5,11-methano-5,6,11,12-tetrahydrodibenzo[b,f][1,5]diazocine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(2-amino-5-methylbenzoyl)-8-amino-2-methyl-5,11-methano-5,6,11,12-tetrahydrodibenzo[b,f][1,5]diazocine

There total 4 articles about N-(2-amino-5-methylbenzoyl)-8-amino-2-methyl-5,11-methano-5,6,11,12-tetrahydrodibenzo[b,f][1,5]diazocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 334874-37-2
N-(5-methyl-2-nitrobenzoyl)-8-amino-2-methyl-5,11-methano-5,6,11,12-tetrahydrodibenzo[b,f][1,5]diazocine

: 334874-40-7
N-(2-amino-5-methylbenzoyl)-8-amino-2-methyl-5,11-methano-5,6,11,12-tetrahydrodibenzo[b,f][1,5]diazocine

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; chloroform; at 20 ℃; for 3h; under 1520.1 Torr;
DOI:10.1021/jo0010882

Reference yield:

: 3113-72-2
5-methyl-2-nitrobenzoic acid

: 334874-40-7
N-(2-amino-5-methylbenzoyl)-8-amino-2-methyl-5,11-methano-5,6,11,12-tetrahydrodibenzo[b,f][1,5]diazocine

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / dicyclohexylcarbodiimide / dimethylformamide / 5 h / 20 °C

2: 98 percent / H₂ / Pd/C / ethanol; CHCl₃ / 3 h / 20 °C / 1520.1 Torr

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In ethanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jo0010882

Reference yield:

: 334874-35-0
8-amino-2-methyl-5,11-methano-5,6,11,12-tetrahydrodibenzo[b,f][1,5]diazocine

: 334874-40-7
N-(2-amino-5-methylbenzoyl)-8-amino-2-methyl-5,11-methano-5,6,11,12-tetrahydrodibenzo[b,f][1,5]diazocine

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / dicyclohexylcarbodiimide / dimethylformamide / 5 h / 20 °C

2: 98 percent / H₂ / Pd/C / ethanol; CHCl₃ / 3 h / 20 °C / 1520.1 Torr

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In ethanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jo0010882