C₄₈H₄₁N₃O₆S₆

Base Information

• Chemical Name: C₄₈H₄₁N₃O₆S₆
• CAS No.: 1228507-87-6
• Molecular Formula: C₄₈H₄₁N₃O₆S₆
• Molecular Weight: 948.266
• Mol file: 1228507-87-6.mol

Synonyms:C₄₈H₄₁N₃O₆S₆

Chemical Property of C₄₈H₄₁N₃O₆S₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₈H₄₁N₃O₆S₆

There total 2 articles about C₄₈H₄₁N₃O₆S₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

1,1,1-tri(hydroxymethyl)propane (77-99-6) + 4-[(pyridine-2-carbothioylsulfanyl)methyl]benzoic acid (1228507-86-5) → C48H41N3O6S6 (1228507-87-6)

Guidance literature:

1,1,1-tri(hydroxymethyl)propane; 4-[(pyridine-2-carbothioylsulfanyl)methyl]benzoic acid; With dmap; 4-(dimethylamino)pyridinium tosylate; In dichloromethane; N,N-dimethyl-formamide; for 0.166667h;

With dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1021/ma100945b

Reference yield:

2-chloromethylpyridine hydrochloride (6959-47-3) → C48H41N3O6S6 (1228507-87-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: tetra-n-propylammonium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 80 °C

2.1: sulfur; potassium tert-butylate / tetrahydrofuran / 12 h / 20 °C

2.2: 5 h / 20 °C

3.1: dmap; 4-(dimethylamino)pyridinium tosylate / dichloromethane; N,N-dimethyl-formamide / 0.17 h

3.2: 20 °C

With sulfur; dmap; potassium tert-butylate; tetra-n-propylammonium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; 4-(dimethylamino)pyridinium tosylate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1021/ma100945b

upstream raw materials:

1,1,1-tri(hydroxymethyl)propane

4-[(pyridine-2-carbothioylsulfanyl)methyl]benzoic acid

2-chloromethylpyridine hydrochloride