1,4,7-Triazacyclononane trihydrobromide

Base Information

• Chemical Name: 1,4,7-Triazacyclononane trihydrobromide
• CAS No.: 35980-59-7
• Molecular Formula: 3Br*C₆H₁₈N₃
• Molecular Weight: 371.941

Synonyms:1,4,7-Triazacyclononane trihydrobromide

Chemical Property of 1,4,7-Triazacyclononane trihydrobromide

Chemical Property:

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MSDS Files:

SDS file from LookChem

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Technology Process of 1,4,7-Triazacyclononane trihydrobromide

There total 1 articles about 1,4,7-Triazacyclononane trihydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

N,N',N-tris(p-toluenesulfonyl)-1,4,7-triazacyclononane (52667-89-7) → N,N'-bis(p-toluenesulfonyl)-1,4,7-triazacyclononane (95388-08-2) + 1-(p-toluenesulfonyl)-1,4,7-triazacyclononane (129422-96-4) + 1,4,7-Triazacyclononane trihydrobromide (35980-59-7)

Guidance literature:

With hydrogen bromide; acetic acid; Heating;

DOI:10.1081/SCC-100105889

Reference yield: 59.0%

1,4,7-Triazacyclononane trihydrobromide (35980-59-7) + ortho-nitrofluorobenzene (1493-27-2,127723-77-7) → 1,4,7-tris(2-nitrophenyl)-1,4,7-triazacyclononane (318501-00-7)

Guidance literature:

With sodium hydroxide; In dichloromethane; water;

DOI:10.1039/b005402j

Reference yield: 58.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 1,4,7-Triazacyclononane trihydrobromide (35980-59-7) → 1,4,7-triazacyclononane-1,4,7-triyl tris(methylenephosphonic acid) (83834-39-3)

Guidance literature:

With hydrogenchloride; phosphonic Acid; at 120 ℃; for 2h;

DOI:10.1007/BF00954193

upstream raw materials:

N,N',N-tris(p-toluenesulfonyl)-1,4,7-triazacyclononane

Downstream raw materials:

1,4,7-triazacyclononane-N,N',N''-triacetic acid trihydrochloride

1,4,7-triazacyclononane-1,4,7-triyl tris(methylenephosphonic acid)

1,4,7-triazacyclononane

1,4,7-tris(2-nitrophenyl)-1,4,7-triazacyclononane

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