O^'4,O⁴-(2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl) 1-di-tert-butyl bis(piperidine-1,4-dicarboxylate)

Base Information

• Chemical Name: O^'4,O⁴-(2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl) 1-di-tert-butyl bis(piperidine-1,4-dicarboxylate)
• CAS No.: 1443300-68-2
• Molecular Formula: C₃₉H₅₅N₅O₁₁
• Molecular Weight: 769.893

Synonyms:O^'4,O⁴-(2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl) 1-di-tert-butyl bis(piperidine-1,4-dicarboxylate)

Chemical Property of O^'4,O⁴-(2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl) 1-di-tert-butyl bis(piperidine-1,4-dicarboxylate)

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Technology Process of O^'4,O⁴-(2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl) 1-di-tert-butyl bis(piperidine-1,4-dicarboxylate)

There total 1 articles about O^'4,O⁴-(2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl) 1-di-tert-butyl bis(piperidine-1,4-dicarboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

3,4-dihydroxy-1-(4-methoxyphenyl)-N2,N2,N5,N5-tetramethyl-1H-pyrrole-2,5-dicarboxamide (1443052-72-9) + N-[(tert-butoxy)carbonyl]piperidine-4-carboxylic acid (84358-13-4,174286-31-8) → O'4,O4-(2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl) 1-di-tert-butyl bis(piperidine-1,4-dicarboxylate) (1443300-68-2)

Guidance literature:

With dmap; diisopropyl-carbodiimide; In ethyl acetate; at 20 ℃; for 2h;

Reference yield: 58.0%

O'4,O4-(2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl) 1-di-tert-butyl bis(piperidine-1,4-dicarboxylate) (1443300-68-2) + trifluoroacetic acid (76-05-1) → 4,4'-(((2,5-bis(dimethylcarbamoyl)-1-(4-methoxyphenyl)-1H-pyrrole-3,4-diyl)bis(oxy))bis(carbonyl))bis(piperidin-1-ium) 2,2,2-trifluoroacetate

Guidance literature:

In dichloromethane; at 20 ℃; for 2h;

upstream raw materials:

3,4-dihydroxy-1-(4-methoxyphenyl)-N²,N²,N⁵,N⁵-tetramethyl-1H-pyrrole-2,5-dicarboxamide

N-[(tert-butoxy)carbonyl]piperidine-4-carboxylic acid

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