S-cinnamyl 2-cyanoethanethioate

Base Information

Chemical Name:S-cinnamyl 2-cyanoethanethioate
CAS No.:1579955-76-2
Molecular Formula:C₁₂H₁₁NOS
Molecular Weight:217.291
Hs Code.:

Synonyms:S-cinnamyl 2-cyanoethanethioate

Suppliers and Price of S-cinnamyl 2-cyanoethanethioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S-cinnamyl 2-cyanoethanethioate

Chemical Property:

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Technology Process of S-cinnamyl 2-cyanoethanethioate

There total 3 articles about S-cinnamyl 2-cyanoethanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 95351-73-8
3-phenyl-prop-2-ene-1-thiol

: 372-09-8
cyanoacetic acid

: 1579955-76-2
S-cinnamyl 2-cyanoethanethioate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.ejmech.2014.01.049

Reference yield:

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 1579955-76-2
S-cinnamyl 2-cyanoethanethioate

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2.17 h / 0 - 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 20 °C

3: dicyclohexyl-carbodiimide; dmap / dichloromethane / 0 - 20 °C

With dmap; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; dicyclohexyl-carbodiimide; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.ejmech.2014.01.049

Reference yield:

: 226090-89-7
S-[(2E)-3-phenylprop-2-en-1-yl]ethanthioate

: 1579955-76-2
S-cinnamyl 2-cyanoethanethioate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 20 °C

2: dicyclohexyl-carbodiimide; dmap / dichloromethane / 0 - 20 °C

With dmap; lithium aluminium tetrahydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.ejmech.2014.01.049