1-(2-benzo[1,3]dioxol-5-yl-3,4,5-trimethoxy-phenyl)-2-methyl-but-3-en-1-ol

Base Information

Chemical Name:1-(2-benzo[1,3]dioxol-5-yl-3,4,5-trimethoxy-phenyl)-2-methyl-but-3-en-1-ol
CAS No.:870283-54-8
Molecular Formula:C₂₁H₂₄O₆
Molecular Weight:372.418
Hs Code.:

Synonyms:1-(2-benzo[1,3]dioxol-5-yl-3,4,5-trimethoxy-phenyl)-2-methyl-but-3-en-1-ol

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Chemical Property of 1-(2-benzo[1,3]dioxol-5-yl-3,4,5-trimethoxy-phenyl)-2-methyl-but-3-en-1-ol

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Technology Process of 1-(2-benzo[1,3]dioxol-5-yl-3,4,5-trimethoxy-phenyl)-2-methyl-but-3-en-1-ol

There total 1 articles about 1-(2-benzo[1,3]dioxol-5-yl-3,4,5-trimethoxy-phenyl)-2-methyl-but-3-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 74199-04-5
4,5,6-trimethoxy-3',4'-mehylendioxybiphenyl-2-carbaldehyde

: 4784-77-4,39616-19-8,29576-14-5
(E)-1-Bromo-2-butene

: 870283-54-8
1-(2-benzo[1,3]dioxol-5-yl-3,4,5-trimethoxy-phenyl)-2-methyl-but-3-en-1-ol

Guidance literature:: With ammonium chloride; zinc; In tetrahydrofuran; water; at 0 ℃; for 1h;
DOI:10.1021/jo0516234

Reference yield:

: 870283-54-8
1-(2-benzo[1,3]dioxol-5-yl-3,4,5-trimethoxy-phenyl)-2-methyl-but-3-en-1-ol

: 1-(2-benzo[1,3]dioxol-5-yl-3,4,5-trimethoxy-phenyl)-2-methyl-butane-1,4-diol

Guidance literature:: 1-(2-benzo[1,3]dioxol-5-yl-3,4,5-trimethoxy-phenyl)-2-methyl-but-3-en-1-ol; With dimethylsulfide borane complex; In tetrahydrofuran; at 20 ℃; for 4h;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; ethanol; water; at 20 ℃; for 3h;
DOI:10.1021/jo0516234

Reference yield:

: 870283-54-8
1-(2-benzo[1,3]dioxol-5-yl-3,4,5-trimethoxy-phenyl)-2-methyl-but-3-en-1-ol

: (4R,5R)-5-(2-Benzo[1,3]dioxol-5-yl-3,4,5-trimethoxy-phenyl)-4-methyl-dihydro-furan-2-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: BH₃*SMe₂ / tetrahydrofuran / 4 h / 20 °C

1.2: H₂O₂; NaOH / tetrahydrofuran; H₂O; ethanol / 3 h / 20 °C

2.1: 37 percent / PPTS / CH₂Cl₂ / 4 h / 20 °C

3.1: 91 percent / PPTS; MeOH / 5 h / 20 °C

4.1: 85 percent / TEMPO; N-chlorosuccinimide; n-Bu₄NI / NaHCO₃; K₂CO₃ / H₂O; CH₂Cl₂ / 3 h / 20 °C

With methanol; 2,2,6,6-tetramethyl-piperidine-N-oxyl; N-chloro-succinimide; dimethylsulfide borane complex; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; potassium carbonate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jo0516234