C₃₇H₅₆O₈Si

Base Information

• Chemical Name: C₃₇H₅₆O₈Si
• CAS No.: 532402-99-6
• Molecular Formula: C₃₇H₅₆O₈Si
• Molecular Weight: 656.932
• Mol file: 532402-99-6.mol

Synonyms:C₃₇H₅₆O₈Si

Chemical Property of C₃₇H₅₆O₈Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₇H₅₆O₈Si

There total 6 articles about C₃₇H₅₆O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

C37H56O7Si (532402-98-5) → C37H56O8Si (532402-99-6)

Guidance literature:

With tert.-butylhydroperoxide; palladium diacetate; In decane; toluene; at 70 ℃; for 20h;

DOI:10.1002/ejoc.200390109

Reference yield:

triethylsilyl chloride (994-30-9) → C37H56O8Si (532402-99-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / imidazole / dimethylformamide / 2 h

2: 35 percent / tBuOOH; Pd(OAc)2 / toluene; decane / 20 h / 70 °C

With 1H-imidazole; tert.-butylhydroperoxide; palladium diacetate; In decane; N,N-dimethyl-formamide; toluene;

DOI:10.1002/ejoc.200390109

Reference yield:

C30H36O7 (532402-91-8) → C37H56O8Si (532402-99-6)

Guidance literature:

Multi-step reaction with 5 steps

1: 77 percent / NaBH₄ / methanol / 1 h / 0 °C

2: 69 percent / NaH / tetrahydrofuran / 3 h / 0 °C

3: 73 percent / CeCl₃*7H₂O; NaBH₄ / methanol / 0.5 h / 0 °C

4: 97 percent / imidazole / dimethylformamide / 2 h

5: 35 percent / tBuOOH; Pd(OAc)2 / toluene; decane / 20 h / 70 °C

With 1H-imidazole; tert.-butylhydroperoxide; palladium diacetate; sodium tetrahydroborate; cerium(III) chloride; sodium hydride; In tetrahydrofuran; methanol; decane; N,N-dimethyl-formamide; toluene;

DOI:10.1002/ejoc.200390109

upstream raw materials:

C₃₇H₅₆O₇Si

triethylsilyl chloride

C₃₀H₃₆O₇

C₃₁H₄₀O₇

Downstream raw materials:

C₃₁H₄₂O₈

C₅₃H₆₉NO₁₁Si