mesityl(3-(methoxycarbonyl)phenyl)iodonium trifluoromethanesulfonate

Base Information

Chemical Name:mesityl(3-(methoxycarbonyl)phenyl)iodonium trifluoromethanesulfonate
CAS No.:1333469-82-1
Molecular Formula:CF₃O₃S*C₁₇H₁₈IO₂
Molecular Weight:530.304
Hs Code.:

Synonyms:mesityl(3-(methoxycarbonyl)phenyl)iodonium trifluoromethanesulfonate

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Chemical Property of mesityl(3-(methoxycarbonyl)phenyl)iodonium trifluoromethanesulfonate

Chemical Property:

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Technology Process of mesityl(3-(methoxycarbonyl)phenyl)iodonium trifluoromethanesulfonate

There total 4 articles about mesityl(3-(methoxycarbonyl)phenyl)iodonium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1493-13-6
trifluorormethanesulfonic acid

: 618-91-7
methyl 3-iodo-benzoate

: 108-67-8
1,3,5-trimethyl-benzene

: 1333469-82-1
mesityl(3-(methoxycarbonyl)phenyl)iodonium trifluoromethanesulfonate

Guidance literature:: With Oxone; In dichloromethane; acetonitrile; at 0 - 20 ℃; for 17h;
DOI:10.1002/chem.201902955

Reference yield:

: 99769-19-4
[3-(methoxycarbonyl)phenyl]boronic acid

: 1333469-82-1
mesityl(3-(methoxycarbonyl)phenyl)iodonium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetonitrile; water / 20 °C

1.2: 20 °C / Heating

2.1: acetonitrile / 1 h / 65 °C

3.1: water; dichloromethane

In dichloromethane; water; acetonitrile;
DOI:10.1039/d1cc06341c

Reference yield:

: 1242733-94-3
potassium (meta-methoxycarbonylphenyl)trifluoroborate

: 33035-41-5
2-(diacetoxyiodo)mesitylene

: 1333469-82-1
mesityl(3-(methoxycarbonyl)phenyl)iodonium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 1 h / 65 °C

2: water; dichloromethane

In dichloromethane; water; acetonitrile;
DOI:10.1039/d1cc06341c