3,5-dichlorophenyl benzyl thioether

Base Information

Chemical Name:3,5-dichlorophenyl benzyl thioether
CAS No.:102871-54-5
Molecular Formula:C₁₃H₁₀Cl₂S
Molecular Weight:269.194
Hs Code.:

Synonyms:3,5-dichlorophenyl benzyl thioether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-dichlorophenyl benzyl thioether

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Technology Process of 3,5-dichlorophenyl benzyl thioether

There total 3 articles about 3,5-dichlorophenyl benzyl thioether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.7%

: 108-70-3,63697-19-8
1,3,5-trichlorobenzene

: 100-53-8
phenylmethanethiol

: 102871-54-5
3,5-dichlorophenyl benzyl thioether

Guidance literature:: With 1,2,3-Benzotriazole; copper(l) iodide; potassium tert-butylate; In dimethyl sulfoxide; at 40 - 100 ℃; for 16h;

Reference yield: 55.0%

: 100-53-8
phenylmethanethiol

: 541-73-1
1,3-Dichlorobenzene

: 102871-54-5
3,5-dichlorophenyl benzyl thioether

Guidance literature:: 1,3-Dichlorobenzene; With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; bis(pinacol)diborane; 4,4'-di-tert-butyl-2,2'-bipyridine; In tert-butyl methyl ether; at 80 ℃; for 1h; Inert atmosphere; Glovebox; Microwave irradiation;

phenylmethanethiol; With pyridine; copper diacetate; In N,N-dimethyl-formamide; at 120 ℃; for 1.5h; regioselective reaction; Inert atmosphere; Microwave irradiation;
DOI:10.1055/s-0033-1339666