2-Chloro-2,4,4,6,6-pentakis-(4-methoxy-phenoxy)-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Base Information

• Chemical Name: 2-Chloro-2,4,4,6,6-pentakis-(4-methoxy-phenoxy)-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine
• CAS No.: 41877-13-8
• Molecular Formula: C₃₅H₃₅ClN₃O₁₀P₃
• Molecular Weight: 786.051

Synonyms:2-Chloro-2,4,4,6,6-pentakis-(4-methoxy-phenoxy)-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Chemical Property of 2-Chloro-2,4,4,6,6-pentakis-(4-methoxy-phenoxy)-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Chemical Property:

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Technology Process of 2-Chloro-2,4,4,6,6-pentakis-(4-methoxy-phenoxy)-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

There total 3 articles about 2-Chloro-2,4,4,6,6-pentakis-(4-methoxy-phenoxy)-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine (940-71-6,16422-79-0) + 4-methoxy-phenol (150-76-5) → 2-Chloro-2,4,4,6,6-pentakis-(4-methoxy-phenoxy)-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (41877-13-8)

Guidance literature:

4-methoxy-phenol; With potassium carbonate; In tetrahydrofuran;

2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; In tetrahydrofuran; at 20 ℃;

DOI:10.1080/10426500802424006

Reference yield: 57.0%

4-methoxy-phenol (150-76-5) → 2-Chloro-2,4,4,6,6-pentakis-(4-methoxy-phenoxy)-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (41877-13-8)

Guidance literature:

With 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 40h;

DOI:10.1039/b702452p

Reference yield:

→ 2-Chloro-2,4,4,6,6-pentakis-(4-methoxy-phenoxy)-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (41877-13-8)

Guidance literature:

p-CH3O-C6H4-OH, Hexachlorocyclotriphosphazotrien, Na;

upstream raw materials:

4-methoxy-phenol

2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine

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