1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic acid

Base Information

Chemical Name:1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic acid
CAS No.:145757-48-8
Molecular Formula:C₁₅H₁₉N₂O₅
Molecular Weight:307.326
Hs Code.:

Synonyms:1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic acid

Suppliers and Price of 1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic acid

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic acid

There total 6 articles about 1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 642097-77-6
1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic ethyl ester

: 145757-48-8
1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic acid

Guidance literature:: With sodium hydroxide; In methanol; at 20 ℃; for 0.5h;
DOI:10.1021/jm050050k

Reference yield:

: 38582-75-1
2-(4-hydroxyphenyl)-4,5-dihydro-4,4,5,5-tetramethyl-3-oxido-3-imidazolio-1-oxyl

: 145757-48-8
1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / sodium ethylate / tetrahydrofuran / 5 h / 60 °C

2: 89 percent / NaOH / H₂O; methanol / 0.5 h / 20 °C

With sodium hydroxide; sodium ethanolate; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.bmc.2006.04.016

Reference yield:

: 14384-45-3
N,N'-dihydroxy-2,3-dimethylbutane-2,3-diamine

: 145757-48-8
1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 51 percent / methanol / 1 h / 20 °C

2: 52 percent / lead dioxide / methanol / 3 h / 20 °C

3: 90 percent / sodium ethylate / tetrahydrofuran / 5 h / 60 °C

4: 89 percent / NaOH / H₂O; methanol / 0.5 h / 20 °C

With sodium hydroxide; sodium ethanolate; lead dioxide; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.bmc.2006.04.016