1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic ethyl ester

Base Information

Chemical Name:1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic ethyl ester
CAS No.:642097-77-6
Molecular Formula:C₁₇H₂₃N₂O₅
Molecular Weight:335.38
Hs Code.:

Synonyms:1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic ethyl ester

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Chemical Property of 1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic ethyl ester

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Technology Process of 1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic ethyl ester

There total 4 articles about 1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 38582-75-1
2-(4-hydroxyphenyl)-4,5-dihydro-4,4,5,5-tetramethyl-3-oxido-3-imidazolio-1-oxyl

: 105-36-2
ethyl bromoacetate

: 642097-77-6
1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic ethyl ester

Guidance literature:: With sodium ethanolate; In tetrahydrofuran; at 60 ℃; for 5h;
DOI:10.1016/j.bmc.2006.04.016

Reference yield:

: 14384-45-3
N,N'-dihydroxy-2,3-dimethylbutane-2,3-diamine

: 642097-77-6
1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 51 percent / methanol / 1 h / 20 °C

2: 52 percent / lead dioxide / methanol / 3 h / 20 °C

3: 90 percent / sodium ethylate / tetrahydrofuran / 5 h / 60 °C

With sodium ethanolate; lead dioxide; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmc.2006.04.016

Reference yield:

: 3964-18-9
2,3-dimethyl-2,3-dinitrobutane

: 642097-77-6
1-(1',3'-dioxyl-4',4',5',5'-tetramethyldihydroimidazol-2'-yl)-phenyl-4-yloxylacetic ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 63 percent / Zn; NH₄Cl / tetrahydrofuran; H₂O / 19 h / 4 - 10 °C

2: 51 percent / methanol / 1 h / 20 °C

3: 52 percent / lead dioxide / methanol / 3 h / 20 °C

4: 90 percent / sodium ethylate / tetrahydrofuran / 5 h / 60 °C

With sodium ethanolate; ammonium chloride; lead dioxide; zinc; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.bmc.2006.04.016