methyl 4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)-butyrate

Base Information

Chemical Name:methyl 4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)-butyrate
CAS No.:88775-50-2
Molecular Formula:C₂₁H₂₂O₈
Molecular Weight:402.401
Hs Code.:

Synonyms:methyl 4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)-butyrate

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Chemical Property of methyl 4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)-butyrate

Chemical Property:

Purity/Quality:

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Technology Process of methyl 4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)-butyrate

There total 4 articles about methyl 4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)-butyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88775-41-1
4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)butyramide

: 1916-07-0
3,4,5-trimethoxybenzoic acid methyl ester

: 88755-16-2
3,4,5-trimethoxybenzoylformic acid

: 88775-51-3
methyl (Z)-2-(3,4,5-trimethoxyphenyl)-4-(3,4-methylenedioxyphenyl)-4-oxo-2-butenoic acid

: 88775-50-2
methyl 4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)-butyrate

Guidance literature:: With sodium hydroxide; potassium carbonate; dimethyl sulfate; Yield given. Multistep reaction. Yields of byproduct given; 1.) aq. EtOH, reflux, 10 h; 2.) acetone, rt., 4 h;
DOI:10.1248/cpb.31.3039

Reference yield:

: 88775-41-1
4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)butyramide

: 77-78-1
dimethyl sulfate

: 1916-07-0
3,4,5-trimethoxybenzoic acid methyl ester

: 88755-16-2
3,4,5-trimethoxybenzoylformic acid

: 88775-51-3
methyl (Z)-2-(3,4,5-trimethoxyphenyl)-4-(3,4-methylenedioxyphenyl)-4-oxo-2-butenoic acid

: 88775-50-2
methyl 4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)-butyrate

Guidance literature:: With sodium hydroxide; potassium carbonate; Yield given. Multistep reaction. Yields of byproduct given; 1.) aq. EtOH, reflux, 10 h; 2.) acetone, rt., 4 h;
DOI:10.1248/cpb.31.3039

Reference yield:

: 88775-24-0
4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)butyronitrile

: 88775-50-2
methyl 4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)-butyrate

Guidance literature:: Multi-step reaction with 2 steps

1: 0.08 g / NaOH / aq. ethanol / 11 h / Heating

2: 1.52 g / K₂CO₃ / acetone / 4 h / Ambient temperature

With sodium hydroxide; potassium carbonate; In ethanol; acetone;
DOI:10.1248/cpb.31.3039