Technology Process of 1-Pyrenebutylamine
There total 6 articles about 1-Pyrenebutylamine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dimethylsulfide borane complex;
In
tetrahydrofuran;
for 1.5h;
Heating;
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
ethanol;
at 20 ℃;
for 48h;
DOI:10.3390/molecules26165032
- Guidance literature:
-
Multi-step reaction with 3 steps
1: oxalyl chloride; DMF / CH2Cl2 / 0.58 h / 20 °C
2: NH3 / CH2Cl2; dioxane / 1.5 h
3: 493 mg / LiAlH4 / tetrahydrofuran / 3 h / 20 °C
With
lithium aluminium tetrahydride; oxalyl dichloride; ammonia; N,N-dimethyl-formamide;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1021/ja057449i
