(R)-2-((1S,2S)-1-Benzyloxy-2-methyl-but-3-enyl)-1,4-dioxa-spiro[4.5]decane

Base Information

Chemical Name:(R)-2-((1S,2S)-1-Benzyloxy-2-methyl-but-3-enyl)-1,4-dioxa-spiro[4.5]decane
CAS No.:1037578-35-0
Molecular Formula:C₂₀H₂₈O₃
Molecular Weight:316.441
Hs Code.:

Synonyms:(R)-2-((1S,2S)-1-Benzyloxy-2-methyl-but-3-enyl)-1,4-dioxa-spiro[4.5]decane

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Chemical Property of (R)-2-((1S,2S)-1-Benzyloxy-2-methyl-but-3-enyl)-1,4-dioxa-spiro[4.5]decane

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Technology Process of (R)-2-((1S,2S)-1-Benzyloxy-2-methyl-but-3-enyl)-1,4-dioxa-spiro[4.5]decane

There total 1 articles about (R)-2-((1S,2S)-1-Benzyloxy-2-methyl-but-3-enyl)-1,4-dioxa-spiro[4.5]decane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 100-39-0
benzyl bromide

: 181139-28-6
(2R,3S,4S)-1,2-cyclohexylidenedioxy-4-methylhex-5-en-3-ol

: 1037578-35-0
(R)-2-((1S,2S)-1-Benzyloxy-2-methyl-but-3-enyl)-1,4-dioxa-spiro[4.5]decane

Guidance literature:: With sodium hydride; In tetrahydrofuran; Heating;
DOI:10.1016/j.tetlet.2008.04.058

Reference yield: 88.0%

: 1037578-35-0
(R)-2-((1S,2S)-1-Benzyloxy-2-methyl-but-3-enyl)-1,4-dioxa-spiro[4.5]decane

: 115408-60-1
(2R,3S,4S)-4-methyl-3-(phenylmethoxy)-5-hexene-1,2-diol

Guidance literature:: With hydrogenchloride; In methanol;
DOI:10.1016/j.tetlet.2008.04.058

Reference yield:

: 1037578-35-0
(R)-2-((1S,2S)-1-Benzyloxy-2-methyl-but-3-enyl)-1,4-dioxa-spiro[4.5]decane

: 328074-86-8
(3S,4S)-3-benzyloxy-4-methyl-hex-1,5-diene

Guidance literature:: Multi-step reaction with 3 steps

1: 2.68 percent / trifluoroacetic acid / H₂O / 6 h / 0 °C

2: 83.6 percent / Et₃N / CH₂Cl₂ / 4 h / 0 °C

3: 51.2 percent / Zn; NaI / dimethylformamide / 5 h / 140 °C

With triethylamine; trifluoroacetic acid; sodium iodide; zinc; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.3390/50801051