3-(6-methoxy-2-naphthyl)-N-(4-methoxyphenyl)-5-nitrobenzamide

Base Information

• Chemical Name: 3-(6-methoxy-2-naphthyl)-N-(4-methoxyphenyl)-5-nitrobenzamide
• CAS No.: 1041114-96-8
• Molecular Formula: C₂₅H₂₀N₂O₅
• Molecular Weight: 428.444
• Mol file: 1041114-96-8.mol

Synonyms:3-(6-methoxy-2-naphthyl)-N-(4-methoxyphenyl)-5-nitrobenzamide

Chemical Property of 3-(6-methoxy-2-naphthyl)-N-(4-methoxyphenyl)-5-nitrobenzamide

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 3-(6-methoxy-2-naphthyl)-N-(4-methoxyphenyl)-5-nitrobenzamide

There total 1 articles about 3-(6-methoxy-2-naphthyl)-N-(4-methoxyphenyl)-5-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

3-(6-methoxy-2-naphthyl)-5-nitrobenzoic acid (1041114-84-4) + 4-methoxy-aniline (104-94-9) → 3-(6-methoxy-2-naphthyl)-N-(4-methoxyphenyl)-5-nitrobenzamide (1041114-96-8)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/jm800367k

Reference yield: 51.0%

3-(6-methoxy-2-naphthyl)-N-(4-methoxyphenyl)-5-nitrobenzamide (1041114-96-8) → 3-(6-hydroxy-2-naphthyl)-N-(4-hydroxyphenyl)-5-nitrobenzamide (1041113-62-5)

Guidance literature:

With boron tribromide; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1021/jm800367k

upstream raw materials:

3-(6-methoxy-2-naphthyl)-5-nitrobenzoic acid

4-methoxy-aniline

Downstream raw materials:

3-(6-hydroxy-2-naphthyl)-N-(4-hydroxyphenyl)-5-nitrobenzamide