(3S)-3-([(1,1-dimethylethyl)oxy]carbonylamino)-1-(methylsulfanyl)-2-oxo-4-phenylbutyl ethanoate

Base Information

Chemical Name:(3S)-3-([(1,1-dimethylethyl)oxy]carbonylamino)-1-(methylsulfanyl)-2-oxo-4-phenylbutyl ethanoate
CAS No.:1393955-00-4
Molecular Formula:C₁₈H₂₅NO₅S
Molecular Weight:367.466
Hs Code.:

Synonyms:(3S)-3-([(1,1-dimethylethyl)oxy]carbonylamino)-1-(methylsulfanyl)-2-oxo-4-phenylbutyl ethanoate

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Chemical Property of (3S)-3-([(1,1-dimethylethyl)oxy]carbonylamino)-1-(methylsulfanyl)-2-oxo-4-phenylbutyl ethanoate

Chemical Property:

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Technology Process of (3S)-3-([(1,1-dimethylethyl)oxy]carbonylamino)-1-(methylsulfanyl)-2-oxo-4-phenylbutyl ethanoate

There total 1 articles about (3S)-3-([(1,1-dimethylethyl)oxy]carbonylamino)-1-(methylsulfanyl)-2-oxo-4-phenylbutyl ethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 184537-67-5
1,1-dimethylethyl N-[(1S)-3-(methylsulfinyl)-2-oxo-1-(phenylmethyl)propyl]carbamate

: 75-36-5
acetyl chloride

: 1393955-00-4
(3S)-3-([(1,1-dimethylethyl)oxy]carbonylamino)-1-(methylsulfanyl)-2-oxo-4-phenylbutyl ethanoate

Guidance literature:: 1,1-dimethylethyl N-[(1S)-3-(methylsulfinyl)-2-oxo-1-(phenylmethyl)propyl]carbamate; With hydrogenchloride; dimethyl sulfoxide; In water; at 20 - 30 ℃; for 4h; Inert atmosphere;

With ammonium hydroxide; In water; at 0 - 10 ℃;

acetyl chloride; With pyridine; In ethyl acetate; at 0 - 30 ℃; for 3h; Inert atmosphere;

Reference yield:

: 1393955-00-4
(3S)-3-([(1,1-dimethylethyl)oxy]carbonylamino)-1-(methylsulfanyl)-2-oxo-4-phenylbutyl ethanoate

: 98760-08-8,98818-34-9,98818-35-0,103127-56-6,98737-29-2
(1-oxiranyl-2-phenylethyl)carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; sodium tetrahydroborate / ethanol / 1 h / -8 - 5 °C / Inert atmosphere

2.1: sodium methylate / methanol / 2 h / 20 - 30 °C / Inert atmosphere

3.1: triethylamine; p-toluenesulfonyl chloride / di(n-butyl)tin oxide / 1-methyl-pyrrolidin-2-one / 1 h / 20 - 30 °C / Inert atmosphere

3.2: 1 h / 20 - 30 °C / Inert atmosphere

With sodium tetrahydroborate; water; sodium methylate; triethylamine; p-toluenesulfonyl chloride; di(n-butyl)tin oxide; In 1-methyl-pyrrolidin-2-one; methanol; ethanol;

Reference yield:

: 1393955-00-4
(3S)-3-([(1,1-dimethylethyl)oxy]carbonylamino)-1-(methylsulfanyl)-2-oxo-4-phenylbutyl ethanoate

: 98760-08-8
(2R,3S)-3-[N-(tert-butyloxycarbonyl)amino]-1,2-epoxy-4-phenylbutane

Guidance literature:: Multi-step reaction with 3 steps

1: water; sodium tetrahydroborate / ethanol / 1 h / -8 - 5 °C / Inert atmosphere

2: dmap; triethylamine / dichloromethane / 1 h / 0 - 30 °C / Inert atmosphere

3: potassium carbonate / tetrahydrofuran; methanol / 15 h / 20 - 30 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; water; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane;