C₆H₃(C₈H₆CN)2CHO

Base Information

Chemical Name:C₆H₃(C₈H₆CN)2CHO
CAS No.:363622-79-1
Molecular Formula:C₂₅H₁₆N₂O
Molecular Weight:360.415
Hs Code.:

C<sub>6</sub>H<sub>3</sub>(C<sub>8</sub>H<sub>6</sub>CN)2CHO

Synonyms:C₆H₃(C₈H₆CN)2CHO

Suppliers and Price of C₆H₃(C₈H₆CN)2CHO

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆H₃(C₈H₆CN)2CHO

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆H₃(C₈H₆CN)2CHO

There total 7 articles about C₆H₃(C₈H₆CN)2CHO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 363622-63-3
C₆H₃(C₈H₆NC)2CH₂OH

: 363622-79-1
C₆H₃(C₈H₆CN)2CHO

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; for 1h;
DOI:10.1021/jo015764r

Reference yield:

: 18226-42-1
1,3,5-Tris(bromomethyl)benzene

: 363622-79-1
C₆H₃(C₈H₆CN)2CHO

Guidance literature:: Multi-step reaction with 5 steps

1: 33 percent / dimethylformamide / 3 h / 100 °C

2: 100 percent / 4 h / 140 °C

3: t-BuOK / tetrahydrofuran / 2 h / 20 °C

4: aq. NaOH / 2 h / 20 °C

5: 91 percent / PCC / CH₂Cl₂ / 1 h

With sodium hydroxide; potassium tert-butylate; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 2: Arbuzov reaction / 3: Horner-Wadsworth-Emmons reaction;
DOI:10.1021/jo015764r

Reference yield:

: 4464-18-0
1,3,5-tris(hydroxymethyl)benzene

: 363622-79-1
C₆H₃(C₈H₆CN)2CHO

Guidance literature:: Multi-step reaction with 6 steps

1: 90 percent / aq. HBr / acetic acid / 1 h / 20 °C

2: 33 percent / dimethylformamide / 3 h / 100 °C

3: 100 percent / 4 h / 140 °C

4: t-BuOK / tetrahydrofuran / 2 h / 20 °C

5: aq. NaOH / 2 h / 20 °C

6: 91 percent / PCC / CH₂Cl₂ / 1 h

With sodium hydroxide; potassium tert-butylate; hydrogen bromide; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; acetic acid; N,N-dimethyl-formamide; 3: Arbuzov reaction / 4: Horner-Wadsworth-Emmons reaction;
DOI:10.1021/jo015764r