C₁₃H₁₂ClN₃O₂

Base Information

Chemical Name:C₁₃H₁₂ClN₃O₂
CAS No.:1402805-40-6
Molecular Formula:C₁₃H₁₂ClN₃O₂
Molecular Weight:277.71
Hs Code.:

C<sub>13</sub>H<sub>12</sub>ClN<sub>3</sub>O<sub>2</sub>

Synonyms:C₁₃H₁₂ClN₃O₂

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Chemical Property of C₁₃H₁₂ClN₃O₂

Chemical Property:

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Technology Process of C₁₃H₁₂ClN₃O₂

There total 4 articles about C₁₃H₁₂ClN₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1402805-39-3
C₁₃H₁₃N₃O₃

: 1402805-40-6
C₁₃H₁₂ClN₃O₂

Guidance literature:: C₁₃H₁₃N₃O₃; With trichlorophosphate; In acetonitrile; at 30 - 45 ℃; for 0.333333h; Inert atmosphere;

With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 45 ℃;

With sodium ethanolate; In water; acetonitrile; at 20 - 40 ℃; for 1h;

Reference yield:

: 32122-09-1
ethyl benzyloxyacetate

: 1402805-40-6
C₁₃H₁₂ClN₃O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride; formic acid ethyl ester / tetrahydrofuran; mineral oil / 5 h / 0 - 20 °C / Cooling with ice

1.2: 16 h / 20 °C / Reflux

2.1: sulfuric acid / 3 h / 90 °C

3.1: trichlorophosphate / acetonitrile / 0.33 h / 30 - 45 °C / Inert atmosphere

3.2: 1.5 h / 45 °C

3.3: 35 - 40 °C / Cooling with ice

With sulfuric acid; sodium hydride; formic acid ethyl ester; trichlorophosphate; In tetrahydrofuran; acetonitrile; mineral oil;

Reference yield:

: 100-39-0
benzyl bromide

: 1402805-40-6
C₁₃H₁₂ClN₃O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; mineral oil / 16 h / 0 - 25 °C

2.1: sodium hydride; formic acid ethyl ester / tetrahydrofuran; mineral oil / 5 h / 0 - 20 °C / Cooling with ice

2.2: 16 h / 20 °C / Reflux

3.1: sulfuric acid / 3 h / 90 °C

4.1: trichlorophosphate / acetonitrile / 0.33 h / 30 - 45 °C / Inert atmosphere

4.2: 1.5 h / 45 °C

4.3: 35 - 40 °C / Cooling with ice

With sulfuric acid; tetra-(n-butyl)ammonium iodide; sodium hydride; formic acid ethyl ester; trichlorophosphate; In tetrahydrofuran; acetonitrile; mineral oil;