TETRAHYDROFURAN-2,2,5,5-D4

Base Information

• Chemical Name: TETRAHYDROFURAN-2,2,5,5-D4
• CAS No.: 20665-63-8
• Molecular Formula: C4H4 D4 O
• Molecular Weight: 76.0752
• Mol file: 20665-63-8.mol

Synonyms:TETRAHYDROFURAN-2,2,5,5-D4

Chemical Property of TETRAHYDROFURAN-2,2,5,5-D4

Chemical Property:

• PSA: 9.23000
• LogP: 0.79680

Purity/Quality:

95% ^*data from raw suppliers

Tetrahydrofuran-2,2,5,5-d4 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TETRAHYDROFURAN-2,2,5,5-D4

There total 2 articles about TETRAHYDROFURAN-2,2,5,5-D4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

succinic acid diethyl ester (123-25-1) → 2,2,5,5-tetradeuterotetrahydrofuran (20665-63-8)

Guidance literature:

With lithium aluminium deuteride; diethyl ether; Erhitzen des Reaktionsprodukts mit wasserhaltiger Phosphorsaeure;

DOI:10.1021/jo01091a024

Reference yield:

→ 2,2,5,5-tetradeuterotetrahydrofuran (20665-63-8)

Guidance literature:

1. C4-Dicarbonsaeure-ethylester, LiAlD4 -> C4-Diol; 2.Erhitzen;

DOI:10.1002/oms.1210010309

Reference yield:

2,2,5,5-tetradeuterotetrahydrofuran (20665-63-8) + bis(pinacol)diborane (73183-34-3) → C4(2)H4H3OBO2C2(CH3)4 + 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane (25015-63-8)

Guidance literature:

With catalyst: ((CH₃)3C₆H₃)Ir(BO₂C₂(CH₃)4)3/C₁₆H₁₆N₂; In neat (no solvent);

DOI:10.1021/ja305596v

upstream raw materials:

succinic acid diethyl ester

Downstream raw materials:

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

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