N''-{4-[(10-{[4'-(decyloxy)-1,1'-biphenyl-4-yl]oxy}decyl)oxy]phenyl}-N,N,N',N'-tetramethylguanidinium chloride

Base Information

Chemical Name:N''-{4-[(10-{[4'-(decyloxy)-1,1'-biphenyl-4-yl]oxy}decyl)oxy]phenyl}-N,N,N',N'-tetramethylguanidinium chloride
CAS No.:1620332-92-4
Molecular Formula:C₄₃H₆₅N₃O₃*ClH
Molecular Weight:708.468
Hs Code.:

Synonyms:N''-{4-[(10-{[4'-(decyloxy)-1,1'-biphenyl-4-yl]oxy}decyl)oxy]phenyl}-N,N,N',N'-tetramethylguanidinium chloride

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Chemical Property of N''-{4-[(10-{[4'-(decyloxy)-1,1'-biphenyl-4-yl]oxy}decyl)oxy]phenyl}-N,N,N',N'-tetramethylguanidinium chloride

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Technology Process of N''-{4-[(10-{[4'-(decyloxy)-1,1'-biphenyl-4-yl]oxy}decyl)oxy]phenyl}-N,N,N',N'-tetramethylguanidinium chloride

There total 8 articles about N''-{4-[(10-{[4'-(decyloxy)-1,1'-biphenyl-4-yl]oxy}decyl)oxy]phenyl}-N,N,N',N'-tetramethylguanidinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1620332-91-3
3-[(10-{[4'-(decyloxy)-1,1'-biphenyl-4-yl]oxy}decyl)oxy]aniline

: 56043-45-9,13829-06-6
N,N,N',N'-tetramethylchlorformamidinium chloride

: 1620332-92-4
N''-{4-[(10-{[4'-(decyloxy)-1,1'-biphenyl-4-yl]oxy}decyl)oxy]phenyl}-N,N,N',N'-tetramethylguanidinium chloride

Guidance literature:: With triethylamine; In tetrahydrofuran; dichloromethane; at 20 ℃; for 72h;
DOI:10.1071/CH14376

Reference yield: 91.0%

: 1620332-86-6
4-[(10-{[4'-(decyloxy)-1,1'-biphenyl-4-yl]oxy}decyl)oxy]aniline

: 56043-45-9,13829-06-6
N,N,N',N'-tetramethylchlorformamidinium chloride

: 1620332-92-4
N''-{4-[(10-{[4'-(decyloxy)-1,1'-biphenyl-4-yl]oxy}decyl)oxy]phenyl}-N,N,N',N'-tetramethylguanidinium chloride

Guidance literature:: With triethylamine; In tetrahydrofuran; dichloromethane; at 20 ℃; for 72h;
DOI:10.1071/CH14376

Reference yield:

: 4101-68-2
1,10-dibromodecane

: 1620332-92-4
N''-{4-[(10-{[4'-(decyloxy)-1,1'-biphenyl-4-yl]oxy}decyl)oxy]phenyl}-N,N,N',N'-tetramethylguanidinium chloride

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetonitrile / 17 h / 100 °C

2: potassium carbonate / methanol / 110 °C

3: hydrogenchloride / water; ethanol / 60 h / 100 °C

4: triethylamine / dichloromethane; tetrahydrofuran / 72 h / 20 °C

With hydrogenchloride; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetonitrile;
DOI:10.1071/CH14376