N-[(1α,5α,6α)-3-benzyl-3-azabicyclo[3.1.0]hex-6-yl]-nitrobenzenesulfonamide

Base Information

• Chemical Name: N-[(1α,5α,6α)-3-benzyl-3-azabicyclo[3.1.0]hex-6-yl]-nitrobenzenesulfonamide
• CAS No.: 1003885-00-4
• Molecular Formula: C₁₈H₁₉N₃O₄S
• Molecular Weight: 373.433

Synonyms:N-[(1α,5α,6α)-3-benzyl-3-azabicyclo[3.1.0]hex-6-yl]-nitrobenzenesulfonamide

Chemical Property of N-[(1α,5α,6α)-3-benzyl-3-azabicyclo[3.1.0]hex-6-yl]-nitrobenzenesulfonamide

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Technology Process of N-[(1α,5α,6α)-3-benzyl-3-azabicyclo[3.1.0]hex-6-yl]-nitrobenzenesulfonamide

There total 1 articles about N-[(1α,5α,6α)-3-benzyl-3-azabicyclo[3.1.0]hex-6-yl]-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

(1α,5α,6α)-3-N-benzyl-6-amino-3-aza-bicyclo[3.1.0]hexane (151860-17-2) + 4-Nitrobenzenesulfonyl chloride (98-74-8) → N-[(1α,5α,6α)-3-benzyl-3-azabicyclo[3.1.0]hex-6-yl]-nitrobenzenesulfonamide (1003885-00-4)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 15.25h;

Reference yield: 85.0%

N-[(1α,5α,6α)-3-benzyl-3-azabicyclo[3.1.0]hex-6-yl]-nitrobenzenesulfonamide (1003885-00-4) + (2S)-2-(4-tert-butyl-phenoxy)-3-[4-(2-hydroxyethoxy)phenyl]propionic acid ethyl ester (1003884-36-3) → (2S)-3-(4-{2-[((1α,5α,6α)-3-benzyl-3-azabicyclo[3.1.0]hex-6-yl)-(4-nitrobenzene-sulfonyl)amino]ethoxy}phenyl)-2-(4-tert-butylphenoxy)propionic acid ethyl ester

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In dichloromethane; at 20 ℃; for 2h;

Reference yield: 61.0%

(2S)-2-ethoxy-3-[4-(2-hydroxyethoxy)phenyl]propionic acid ethyl ester (552330-51-5) + N-[(1α,5α,6α)-3-benzyl-3-azabicyclo[3.1.0]hex-6-yl]-nitrobenzenesulfonamide (1003885-00-4) → (2S)-3-(4-{2-[((1α,5α,6α)-3-benzyl-3-azabicyclo[3.1.0]hex-6-yl)-(4-nitrobenzene-sulfonyl)amino]ethoxy}phenyl)-2-ethoxypropionic acid ethyl ester

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In dichloromethane; at 20 ℃; for 2h;

upstream raw materials:

(1α,5α,6α)-3-N-benzyl-6-amino-3-aza-bicyclo[3.1.0]hexane

4-Nitrobenzenesulfonyl chloride

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