(R)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-phenyl-propionic acid methyl ester

Base Information

Chemical Name:(R)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-phenyl-propionic acid methyl ester
CAS No.:145313-30-0
Molecular Formula:C₁₅H₂₂N₂O₃
Molecular Weight:278.351
Hs Code.:

Synonyms:(R)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-phenyl-propionic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-phenyl-propionic acid methyl ester

Chemical Property:

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Technology Process of (R)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-phenyl-propionic acid methyl ester

There total 26 articles about (R)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-phenyl-propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4817-95-2
N-(benzyloxycarbonyl)-L-valyl-L-phenylalanine methyl ester

: 39614-17-0,128557-46-0,145313-30-0
L-valyl-L-phenylalanine methyl ester

Guidance literature:: With hydrogenchloride; hydrogen; palladium; In methanol;

Reference yield:

: 2577-90-4
methyl (2S)-2-amino-3-phenylpropanoate

: 39614-17-0,128557-46-0,145313-30-0
L-valyl-L-phenylalanine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / ethyldiisopropylamine; 2-(1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium BF₄ / CH₂Cl₂ / 20 °C

2: 100 percent / trifluoroacetic acid; anisole / CH₂Cl₂

With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jo061830j

Reference yield:

: 1149-26-4
(S)-N-(benzyloxycarbonyl)valine

: 39614-17-0,128557-46-0,145313-30-0
L-valyl-L-phenylalanine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N, isobutyl chloroformate / tetrahydrofuran / 16 h / Ambient temperature

2: H₂ / 5percent Pd/C / methanol / 5 h / Ambient temperature

With hydrogen; triethylamine; isobutyl chloroformate; palladium on activated charcoal; In tetrahydrofuran; methanol;