2-[4-(diethoxymethyl)phenyl]-1,3-dimethyl-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate

Base Information

Chemical Name:2-[4-(diethoxymethyl)phenyl]-1,3-dimethyl-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate
CAS No.:290297-87-9
Molecular Formula:C₂₃H₂₆N₂O₄
Molecular Weight:394.47
Hs Code.:

Synonyms:2-[4-(diethoxymethyl)phenyl]-1,3-dimethyl-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate

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Chemical Property of 2-[4-(diethoxymethyl)phenyl]-1,3-dimethyl-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate

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Technology Process of 2-[4-(diethoxymethyl)phenyl]-1,3-dimethyl-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate

There total 4 articles about 2-[4-(diethoxymethyl)phenyl]-1,3-dimethyl-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 15781-73-4
di(2,4,6-trichlorophenyl)-2-phenylmalonate

: 290297-86-8
4-(diethoxymethyl)-N,N'-dimethylbenzamidine

: 290297-87-9
2-[4-(diethoxymethyl)phenyl]-1,3-dimethyl-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate

Guidance literature:: In methoxybenzene; for 0.05h; Heating;
DOI:10.1021/ol0060329

Reference yield:

: 623-27-8
terephthalaldehyde,

: 290297-87-9
2-[4-(diethoxymethyl)phenyl]-1,3-dimethyl-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 16 percent / conc. H₂SO₄ / ethanol / 12 h / 20 °C

2.1: 69 percent / sulphur / ethanol / 4 h / 110 °C

3.1: diethyl ether / 70 h / 20 °C

3.2: 83 percent / ethanol / 7.5 h

4.1: 69 percent / methoxybenzene / 0.05 h / Heating

With sulfuric acid; sulfur; In diethyl ether; ethanol; methoxybenzene; 1.1: acetalization / 2.1: Wilgerodt-Kindler reaction / 3.1: Methylation / 3.2: Substitution / 4.1: cyclocondensation;
DOI:10.1021/ol0060329

Reference yield:

: 81172-89-6
terephthalaldehyde mono(diethylacetal)

: 290297-87-9
2-[4-(diethoxymethyl)phenyl]-1,3-dimethyl-5-phenyl-6-oxo-6H-1-pyrimidinium-4-olate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 69 percent / sulphur / ethanol / 4 h / 110 °C

2.1: diethyl ether / 70 h / 20 °C

2.2: 83 percent / ethanol / 7.5 h

3.1: 69 percent / methoxybenzene / 0.05 h / Heating

With sulfur; In diethyl ether; ethanol; methoxybenzene; 1.1: Wilgerodt-Kindler reaction / 2.1: Methylation / 2.2: Substitution / 3.1: cyclocondensation;
DOI:10.1021/ol0060329