(2S,3S)-2-acetyloxy-3-(benzoylamino)-3-phenylpropanoic acid methyl ester

Base Information

Chemical Name:(2S,3S)-2-acetyloxy-3-(benzoylamino)-3-phenylpropanoic acid methyl ester
CAS No.:161060-39-5
Molecular Formula:C₁₉H₁₉NO₅
Molecular Weight:341.364
Hs Code.:

Synonyms:(2S,3S)-2-acetyloxy-3-(benzoylamino)-3-phenylpropanoic acid methyl ester

Suppliers and Price of (2S,3S)-2-acetyloxy-3-(benzoylamino)-3-phenylpropanoic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,3S)-2-acetyloxy-3-(benzoylamino)-3-phenylpropanoic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,3S)-2-acetyloxy-3-(benzoylamino)-3-phenylpropanoic acid methyl ester

There total 7 articles about (2S,3S)-2-acetyloxy-3-(benzoylamino)-3-phenylpropanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 108-05-4,9003-20-7
vinyl acetate

: erythro N-benzoyl-3-phenylisoserine methyl ester

: 161060-39-5
(2S,3S)-2-acetyloxy-3-(benzoylamino)-3-phenylpropanoic acid methyl ester

Guidance literature:: In various solvent(s); for 96h; Ambient temperature; lipase from Pseudomonas Fluorescens;
DOI:10.1016/0040-4020(96)00143-3

Reference yield:

: 140196-38-9
1,1-dimethyl (2-oxo-1-phenylethyl)carbamate

: 161060-39-5
(2S,3S)-2-acetyloxy-3-(benzoylamino)-3-phenylpropanoic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: Et₃N / CH₂Cl₂ / Ambient temperature

2: Et₃N / 36 h / Ambient temperature

3: 1.) 6N aq. HCl, 2.) SOCl₂ / 1.) 110 deg C, 12 h, 2.) RT, 12 h

4: Et₃N, 4-dimethylaminopyridine / CH₂Cl₂ / 0.5 h / Ambient temperature

5: 90 percent / various solvent(s) / 96 h / Ambient temperature; lipase from Pseudomonas Fluorescens

With hydrogenchloride; dmap; thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1016/0040-4020(96)00143-3

Reference yield:

: 161060-38-4
[2-Hydroxy-2-(4-isopropyl-5-oxo-2,5-dihydro-oxazol-2-yl)-1-phenyl-ethyl]-carbamic acid tert-butyl ester

: 161060-39-5
(2S,3S)-2-acetyloxy-3-(benzoylamino)-3-phenylpropanoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / 36 h / Ambient temperature

2: 1.) 6N aq. HCl, 2.) SOCl₂ / 1.) 110 deg C, 12 h, 2.) RT, 12 h

3: Et₃N, 4-dimethylaminopyridine / CH₂Cl₂ / 0.5 h / Ambient temperature

4: 90 percent / various solvent(s) / 96 h / Ambient temperature; lipase from Pseudomonas Fluorescens

With hydrogenchloride; dmap; thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1016/0040-4020(96)00143-3