[5'-DMTr-2'-TBDMS-rU]-[3'-p(OMe)-5']-[rU-2'-TBDMS]-[3'-p(OMe)-5']-[rU-2'-TIPS]-3'-methylphosphoramidite

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Chemical Name:[5'-DMTr-2'-TBDMS-rU]-[3'-p(OMe)-5']-[rU-2'-TBDMS]-[3'-p(OMe)-5']-[rU-2'-TIPS]-3'-methylphosphoramidite
CAS No.:1309673-38-8
Molecular Formula:C₇₈H₁₂₀N₇O₂₅P₃Si₃
Molecular Weight:1733.02
Hs Code.:

Synonyms:[5'-DMTr-2'-TBDMS-rU]-[3'-p(OMe)-5']-[rU-2'-TBDMS]-[3'-p(OMe)-5']-[rU-2'-TIPS]-3'-methylphosphoramidite

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Chemical Property of [5'-DMTr-2'-TBDMS-rU]-[3'-p(OMe)-5']-[rU-2'-TBDMS]-[3'-p(OMe)-5']-[rU-2'-TIPS]-3'-methylphosphoramidite

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Technology Process of [5'-DMTr-2'-TBDMS-rU]-[3'-p(OMe)-5']-[rU-2'-TBDMS]-[3'-p(OMe)-5']-[rU-2'-TIPS]-3'-methylphosphoramidite

There total 1 articles about [5'-DMTr-2'-TBDMS-rU]-[3'-p(OMe)-5']-[rU-2'-TBDMS]-[3'-p(OMe)-5']-[rU-2'-TIPS]-3'-methylphosphoramidite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1309592-60-6
[5'-DMTr-2'-TBDMS-rU]-[3'-p(OMe)-5']-[rU-2'-TBDMS]-[3'-p(OMe)-5']-[rU-2'-TIPS]

: 92611-10-4
bis(N,N-diisopropylamino)methoxyphosphine

: 1309673-38-8
[5'-DMTr-2'-TBDMS-rU]-[3'-p(OMe)-5']-[rU-2'-TBDMS]-[3'-p(OMe)-5']-[rU-2'-TIPS]-3'-methylphosphoramidite

Guidance literature:: bis(N,N-diisopropylamino)methoxyphosphine; With N,N-diisopropylamine tetrazolide; In dichloromethane; Sonication;

[5'-DMTr-2'-TBDMS-rU]-[3'-p(OMe)-5']-[rU-2'-TBDMS]-[3'-p(OMe)-5']-[rU-2'-TIPS]; at 20 ℃; Sonication;
DOI:10.1016/j.tetlet.2011.03.042