3-endo-[8-(2,2,2-trifluoroacetyl)-8-azabicyclo[3.2.1]oct-3-yl]-benzonitrile

Base Information

Chemical Name:3-endo-[8-(2,2,2-trifluoroacetyl)-8-azabicyclo[3.2.1]oct-3-yl]-benzonitrile
CAS No.:949903-29-1
Molecular Formula:C₁₆H₁₅F₃N₂O
Molecular Weight:308.303
Hs Code.:

Synonyms:3-endo-[8-(2,2,2-trifluoroacetyl)-8-azabicyclo[3.2.1]oct-3-yl]-benzonitrile

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Chemical Property of 3-endo-[8-(2,2,2-trifluoroacetyl)-8-azabicyclo[3.2.1]oct-3-yl]-benzonitrile

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Technology Process of 3-endo-[8-(2,2,2-trifluoroacetyl)-8-azabicyclo[3.2.1]oct-3-yl]-benzonitrile

There total 1 articles about 3-endo-[8-(2,2,2-trifluoroacetyl)-8-azabicyclo[3.2.1]oct-3-yl]-benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 949903-28-0
trifluoromethanesulfonic acid 3-endo-[8-(2,2,2-trifluoro-acetyl)-8-azabicyclo[3.2.1]oct-3-yl]phenyl ester

: 557-21-1
dicyanozinc

: 949903-29-1
3-endo-[8-(2,2,2-trifluoroacetyl)-8-azabicyclo[3.2.1]oct-3-yl]-benzonitrile

Guidance literature:: 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In water; N,N-dimethyl-formamide; at 120 ℃; for 4h;

Reference yield:

: 949903-29-1
3-endo-[8-(2,2,2-trifluoroacetyl)-8-azabicyclo[3.2.1]oct-3-yl]-benzonitrile

: 949904-53-4
3-endo-(8-azabicyclo[3.2.1]oct-3-yl)benzamide hydrochloride

Guidance literature:: 3-endo-[8-(2,2,2-trifluoroacetyl)-8-azabicyclo[3.2.1]oct-3-yl]-benzonitrile; With sulfuric acid; water; at 50 ℃; for 2h;

With sodium hydroxide; In methanol; water; at 10 - 22 ℃; for 1h;

With hydrogenchloride; In ethanol; water;

Reference yield:

: 949903-29-1
3-endo-[8-(2,2,2-trifluoroacetyl)-8-azabicyclo[3.2.1]oct-3-yl]-benzonitrile

: 949902-11-8
3-endo-(8-azabicyclo[3.2.1]oct-3-yl)-benzamide

Guidance literature:: 3-endo-[8-(2,2,2-trifluoroacetyl)-8-azabicyclo[3.2.1]oct-3-yl]-benzonitrile; With sulfuric acid; water; at 50 ℃; for 2h;

With sodium hydroxide; In methanol; water; at 10 - 22 ℃; for 1h;