4-(DIFLUOROMETHYLSULFONYL)NITROBENZENE

Base Information

Chemical Name:4-(DIFLUOROMETHYLSULFONYL)NITROBENZENE
CAS No.:24906-74-9
Molecular Formula:C7H5 F2 N O4 S
Molecular Weight:237.184
Hs Code.:2904909090
Mol file:24906-74-9.mol

Synonyms:Sulfone,difluoromethyl p-nitrophenyl (8CI); Difluoromethyl p-nitrophenyl sulfone

Suppliers and Price of 4-(DIFLUOROMETHYLSULFONYL)NITROBENZENE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-(DIFLUOROMETHANE)SULFONYL-4-NITROBENZENE 95.00%
5G
$ 1467.43

Total 5 raw suppliers

Chemical Property of 4-(DIFLUOROMETHYLSULFONYL)NITROBENZENE

Chemical Property:

Boiling Point:386.7±42.0 °C(Predicted)
PSA：88.34000
Density:1.536±0.06 g/cm3(Predicted)
LogP:3.19510

Purity/Quality:

99% ^*data from raw suppliers

1-(DIFLUOROMETHANE)SULFONYL-4-NITROBENZENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 20/21/22-36/37/38
Safety Statements: 23-36/37/39

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-(DIFLUOROMETHYLSULFONYL)NITROBENZENE

There total 5 articles about 4-(DIFLUOROMETHYLSULFONYL)NITROBENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 24933-57-1
1-[(difluoromethyl)thio]-4-nitrobenzene

: 24906-74-9
1-((difluoromethyl)sulfonyl)-4-nitrobenzene

Guidance literature:: With sodium periodate; ruthenium(III) chloride dihydrate; In tetrachloromethane; water; acetonitrile; at 0 - 20 ℃; for 1.5h;
DOI:10.1002/anie.201007594

Reference yield: 61.0%

: 5448-68-0
benzaldehyde p-nitrobenzenesulfonylhydrazone

: 2,2‐difluoro‐2‐(triphenylphosphonio)acetate

: 24906-74-9
1-((difluoromethyl)sulfonyl)-4-nitrobenzene

Guidance literature:: With cesium bicarbonate; In cyclohexane; at 100 ℃; for 6h;
DOI:10.1039/c6ra20629h

Reference yield: 46.0%

: 275818-95-6
sodium difluoromethanesulfinate

: 456-27-9
4-nitrobenzenediazonium tetrafluoroborate

: 24906-74-9
1-((difluoromethyl)sulfonyl)-4-nitrobenzene

Guidance literature:: sodium difluoromethanesulfinate; With copper(I) thiophene-2-carboxylate; In acetonitrile; at 20 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;

4-nitrobenzenediazonium tetrafluoroborate; In acetonitrile; at 20 ℃; for 0.75h; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1002/cjoc.201700748