C₁₃H₁₇NO₅

Base Information

Chemical Name:C₁₃H₁₇NO₅
CAS No.:1280608-82-3
Molecular Formula:C₁₃H₁₇NO₅
Molecular Weight:267.282
Hs Code.:

C<sub>13</sub>H<sub>17</sub>NO<sub>5</sub>

Synonyms:C₁₃H₁₇NO₅

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Chemical Property of C₁₃H₁₇NO₅

Chemical Property:

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Technology Process of C₁₃H₁₇NO₅

There total 7 articles about C₁₃H₁₇NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1280608-81-2
C₁₃H₁₆O₅

: 1280608-82-3
C₁₃H₁₇NO₅

Guidance literature:: With hydroxylamine hydrochloride; potassium carbonate; In methanol; water; at 0 ℃; for 1h;
DOI:10.1002/anie.201006528

Reference yield:

: 705-76-0
3,5-dimethoxybenzyl alcohol

: 1280608-82-3
C₁₃H₁₇NO₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: manganese(IV) oxide / toluene / 15 h / Reflux

2.1: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione / chloroform / 0 - 20 °C

3.1: tetra-N-butylammonium tribromide; orthoformic acid triethyl ester / 0 - 20 °C

4.1: n-butyllithium / tetrahydrofuran; diethyl ether; hexane / -78 °C / Inert atmosphere

4.2: -78 - 0 °C / Inert atmosphere

5.1: hydroxylamine hydrochloride; potassium carbonate / methanol; water / 1 h / 0 °C

With manganese(IV) oxide; n-butyllithium; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; hydroxylamine hydrochloride; tetra-N-butylammonium tribromide; potassium carbonate; orthoformic acid triethyl ester; In tetrahydrofuran; methanol; diethyl ether; hexane; chloroform; water; toluene;
DOI:10.1002/anie.201006528

Reference yield:

: 2150-37-0
methyl 3,5-dimethoxybenzoate

: 1280608-82-3
C₁₃H₁₇NO₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 1.67 h / Reflux

2.1: manganese(IV) oxide / toluene / 15 h / Reflux

3.1: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione / chloroform / 0 - 20 °C

4.1: tetra-N-butylammonium tribromide; orthoformic acid triethyl ester / 0 - 20 °C

5.1: n-butyllithium / tetrahydrofuran; diethyl ether; hexane / -78 °C / Inert atmosphere

5.2: -78 - 0 °C / Inert atmosphere

6.1: hydroxylamine hydrochloride; potassium carbonate / methanol; water / 1 h / 0 °C

With manganese(IV) oxide; sodium tetrahydroborate; n-butyllithium; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; hydroxylamine hydrochloride; tetra-N-butylammonium tribromide; potassium carbonate; orthoformic acid triethyl ester; In tetrahydrofuran; methanol; diethyl ether; hexane; chloroform; water; toluene;
DOI:10.1002/anie.201006528