carbamic acid N-[(dimethoxyphosphinyl)phenylmethyl] 1,1-dimethylethyl ester

Base Information

Chemical Name:carbamic acid N-[(dimethoxyphosphinyl)phenylmethyl] 1,1-dimethylethyl ester
CAS No.:71864-40-9
Molecular Formula:C₁₄H₂₂NO₅P
Molecular Weight:315.306
Hs Code.:

Synonyms:carbamic acid N-[(dimethoxyphosphinyl)phenylmethyl] 1,1-dimethylethyl ester

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Chemical Property of carbamic acid N-[(dimethoxyphosphinyl)phenylmethyl] 1,1-dimethylethyl ester

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Technology Process of carbamic acid N-[(dimethoxyphosphinyl)phenylmethyl] 1,1-dimethylethyl ester

There total 4 articles about carbamic acid N-[(dimethoxyphosphinyl)phenylmethyl] 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 35657-34-2
(O-pivaloylhydroxyl)amine

: 16965-72-3
dimethyl α-diazobenzylphosphonate

: 71864-40-9
carbamic acid N-[(dimethoxyphosphinyl)phenylmethyl] 1,1-dimethylethyl ester

Guidance literature:: rhodium(II) acetate; In toluene; for 1h; Heating;
DOI:10.1039/P19960002879

Reference yield: 94.0%

: 36198-87-5
dimethyl trimethylsilyl phosphite

: 150884-50-7
benzaldehyde N-boc imine

: 71864-40-9
carbamic acid N-[(dimethoxyphosphinyl)phenylmethyl] 1,1-dimethylethyl ester

Guidance literature:: dimethyl trimethylsilyl phosphite; benzaldehyde N-boc imine; In tetrahydrofuran; at 0 - 20 ℃; for 5h; Inert atmosphere;

With water; In tetrahydrofuran; for 0.5h; Inert atmosphere;
DOI:10.1002/cjoc.201200119

Reference yield: 51.0%

: 868-85-9
Dimethyl phosphite

: 150884-50-7
benzaldehyde N-boc imine

: 71864-40-9
carbamic acid N-[(dimethoxyphosphinyl)phenylmethyl] 1,1-dimethylethyl ester

Guidance literature:: With 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene; In tetrahydrofuran; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1055/s-0031-1289690