[(PMe3)4Ru(η2-OAc)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

Base Information

Chemical Name:[(PMe3)4Ru(η2-OAc)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]
CAS No.:1187982-95-1
Molecular Formula:C₁₄H₃₉O₂P₄Ru*C₃₂H₁₂BF₂₄
Molecular Weight:1327.65
Hs Code.:

Synonyms:[(PMe3)4Ru(η2-OAc)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [(PMe3)4Ru(η2-OAc)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

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Technology Process of [(PMe3)4Ru(η2-OAc)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

There total 1 articles about [(PMe3)4Ru(η2-OAc)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1187982-90-6,88968-54-1
cis-[RuCl(CH₃COO)(P(CH₃)3)4]

: 79060-88-1
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

: 1187982-95-1
[(PMe3)4Ru(η2-OAc)][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

Guidance literature:: With MeOH; In methanol; chloroform; byproducts: NaCl; (N2); high-vac. technique; 24% MeOH/CHCl3 was added to soln. of Ru complex in CHCl3; stirred for 20 min; soln. of Na salt in MeOH was added; filtered through glass wool layered with Celite; filtrate concd.; crystd. (pentane); recrystd. (CH2Cl2/pentane, -23°C); elem. anal.;
DOI:10.1021/om900128s