6-(4-tert-butyl-cyclohexyloxy)-1,2,3,4-tetrahydro-isoquinoline hydrochloride

Base Information

Chemical Name:6-(4-tert-butyl-cyclohexyloxy)-1,2,3,4-tetrahydro-isoquinoline hydrochloride
CAS No.:1266120-56-2
Molecular Formula:C₁₉H₂₉NO*ClH
Molecular Weight:323.906
Hs Code.:

Synonyms:6-(4-tert-butyl-cyclohexyloxy)-1,2,3,4-tetrahydro-isoquinoline hydrochloride

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Chemical Property of 6-(4-tert-butyl-cyclohexyloxy)-1,2,3,4-tetrahydro-isoquinoline hydrochloride

Chemical Property:

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Technology Process of 6-(4-tert-butyl-cyclohexyloxy)-1,2,3,4-tetrahydro-isoquinoline hydrochloride

There total 3 articles about 6-(4-tert-butyl-cyclohexyloxy)-1,2,3,4-tetrahydro-isoquinoline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1266120-54-0
6-(4-tert-butyl-cyclohexyloxy)-3,4-dihydro-1H-isoquinoline-2-carboxylic acid tert-butyl ester

: 1266120-56-2
6-(4-tert-butyl-cyclohexyloxy)-1,2,3,4-tetrahydro-isoquinoline hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; diethyl ether; at 20 ℃; for 3h;

Reference yield:

: 63905-73-7
6-hydroxy-1,2,3,4-tetrahydroisoquinoline hydrochloride

: 1266120-56-2
6-(4-tert-butyl-cyclohexyloxy)-1,2,3,4-tetrahydro-isoquinoline hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / chloroform; water / 20 °C

2: caesium carbonate / butanone; tert-butyl alcohol / 100 °C / Sealed tube

3: hydrogenchloride / 1,4-dioxane; diethyl ether / 3 h / 20 °C

With hydrogenchloride; sodium hydrogencarbonate; caesium carbonate; In 1,4-dioxane; diethyl ether; chloroform; water; butanone; tert-butyl alcohol;

Reference yield:

: 158984-83-9
N-tert-butoxycarbonyl-6-hydroxy-1,2,3,4-tetrahydroisoquinoline

: 1266120-56-2
6-(4-tert-butyl-cyclohexyloxy)-1,2,3,4-tetrahydro-isoquinoline hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / butanone; tert-butyl alcohol / 100 °C / Sealed tube

2: hydrogenchloride / 1,4-dioxane; diethyl ether / 3 h / 20 °C

With hydrogenchloride; caesium carbonate; In 1,4-dioxane; diethyl ether; butanone; tert-butyl alcohol;