benzoic acid 1-cyanobutyl ester

Base Information

• Chemical Name: benzoic acid 1-cyanobutyl ester
• CAS No.: 129803-21-0
• Molecular Formula: C₁₂H₁₃NO₂
• Molecular Weight: 203.241
• Mol file: 129803-21-0.mol

Synonyms:benzoic acid 1-cyanobutyl ester

Chemical Property of benzoic acid 1-cyanobutyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of benzoic acid 1-cyanobutyl ester

There total 3 articles about benzoic acid 1-cyanobutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C11H13O2Br + potassium cyanide (151-50-8) → benzoic acid 1-cyanobutyl ester (129803-21-0)

Guidance literature:

In dimethyl sulfoxide; at 20 ℃; for 4h;

DOI:10.1016/j.tet.2007.04.021

Reference yield: 94.0%

benzoyl cyanide (613-90-1) + butyraldehyde (123-72-8) → benzoic acid 1-cyanobutyl ester (129803-21-0)

Guidance literature:

With potassium carbonate; In acetonitrile; for 1h; Ambient temperature;

DOI:10.1055/s-1996-4361

Reference yield:

2-oxopentanenitrile (38576-58-8) + benzaldehyde (100-52-7) → benzoic acid 1-cyanobutyl ester (129803-21-0)

Guidance literature:

With triethylamine; In acetonitrile; at 20 ℃;

DOI:10.1002/adsc.202000125

upstream raw materials:

benzoyl cyanide

butyraldehyde

potassium cyanide

2-oxopentanenitrile