[Cu(I)(2,9-dimethyl-1,10-phenanthroline)(1,2-bis(diphenylphosphino)ethane)][PF₆]

Base Information

• Chemical Name: [Cu(I)(2,9-dimethyl-1,10-phenanthroline)(1,2-bis(diphenylphosphino)ethane)][PF₆]
• CAS No.: 713496-85-6
• Molecular Formula: C₄₀H₃₆CuN₂P₂*F₆P
• Molecular Weight: 815.197

Synonyms:[Cu(I)(2,9-dimethyl-1,10-phenanthroline)(1,2-bis(diphenylphosphino)ethane)][PF₆]

Chemical Property of [Cu(I)(2,9-dimethyl-1,10-phenanthroline)(1,2-bis(diphenylphosphino)ethane)][PF₆]

Chemical Property:

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Technology Process of [Cu(I)(2,9-dimethyl-1,10-phenanthroline)(1,2-bis(diphenylphosphino)ethane)][PF₆]

There total 2 articles about [Cu(I)(2,9-dimethyl-1,10-phenanthroline)(1,2-bis(diphenylphosphino)ethane)][PF₆] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

tetrakis(actonitrile)copper(I) hexafluorophosphate (64443-05-6) + 2.9-dimethyl-1,10-phenanthroline (484-11-7) + 1,2-bis-(diphenylphosphino)ethane (1663-45-2) → [Cu(I)(2,9-dimethyl-1,10-phenanthroline)(1,2-bis(diphenylphosphino)ethane)][PF6] (713496-85-6)

Guidance literature:

In dichloromethane; (Ar); std. Schlenk technique; mixt. of Cu complex, phenanthroline and P ligand in CH2Cl2 was stirred at room temp. for 90 min; Et2O added; filtered; dried (vac.);

DOI:10.1039/b608641a

Reference yield: 70.0%

tetrakis(actonitrile)copper(I) hexafluorophosphate (64443-05-6) + 2,9-dimethyl-1,10-phenanthroline hemihydrate (34302-69-7) + 1,2-bis-(diphenylphosphino)ethane (1663-45-2) → [Cu(I)(2,9-dimethyl-1,10-phenanthroline)(1,2-bis(diphenylphosphino)ethane)][PF6] (713496-85-6)

Guidance literature:

In acetonitrile; (Cu(CH3CN)4)(PF6) was added to soln. dmp*0.5H2O and dppe and refluxed for 2 h; solvent was removed in vacuo, residue was recrystd. from MeCN;

upstream raw materials:

tetrakis(actonitrile)copper(I) hexafluorophosphate

2.9-dimethyl-1,10-phenanthroline

1,2-bis-(diphenylphosphino)ethane

2,9-dimethyl-1,10-phenanthroline hemihydrate

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