Technology Process of C26H34N4O3
There total 6 articles about C26H34N4O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
chloro-trimethyl-silane; sodium iodide;
In
acetonitrile;
at 20 ℃;
for 2h;
DOI:10.1016/j.bmcl.2012.06.022
- Guidance literature:
-
Multi-step reaction with 3 steps
1: water; lithium hydroxide / tetrahydrofuran / 70 °C
2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 20 °C
3: chloro-trimethyl-silane; sodium iodide / acetonitrile / 2 h / 20 °C
With
chloro-trimethyl-silane; water; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; sodium iodide; lithium hydroxide;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2012.06.022
- Guidance literature:
-
Multi-step reaction with 7 steps
1: methanol / 48 h / 10 - 20 °C / Cooling with ice
2: pyridine / 12 h / Reflux
3: potassium carbonate / ethyl acetate / 12 h / 20 °C
4: tetrahydrofuran / 70 °C
5: water; lithium hydroxide / tetrahydrofuran / 70 °C
6: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 20 °C
7: chloro-trimethyl-silane; sodium iodide / acetonitrile / 2 h / 20 °C
With
pyridine; chloro-trimethyl-silane; water; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; sodium iodide; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1016/j.bmcl.2012.06.022
