(Au(P(C₆H₅)3))2(C(CH₃)CHOC₂H₅)⁽¹⁺⁾*N(SO₂CF₃)2^(1-)=[(Au(P(C₆H₅)3))2(C(CH₃)CHOC₂H₅)](N(SO₂CF₃)2)

Base Information

• Chemical Name: (Au(P(C₆H₅)3))2(C(CH₃)CHOC₂H₅)⁽¹⁺⁾*N(SO₂CF₃)2^(1-)=[(Au(P(C₆H₅)3))2(C(CH₃)CHOC₂H₅)](N(SO₂CF₃)2)
• CAS No.: 1259488-31-7
• Molecular Formula: C₂F₆NO₄S₂*C₄₁H₃₉Au₂OP₂
• Molecular Weight: 1283.79

Synonyms:(Au(P(C₆H₅)3))2(C(CH₃)CHOC₂H₅)⁽¹⁺⁾*N(SO₂CF₃)2^(1-)=[(Au(P(C₆H₅)3))2(C(CH₃)CHOC₂H₅)](N(SO₂CF₃)2)

Chemical Property of (Au(P(C₆H₅)3))2(C(CH₃)CHOC₂H₅)⁽¹⁺⁾*N(SO₂CF₃)2^(1-)=[(Au(P(C₆H₅)3))2(C(CH₃)CHOC₂H₅)](N(SO₂CF₃)2)

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Technology Process of (Au(P(C₆H₅)3))2(C(CH₃)CHOC₂H₅)⁽¹⁺⁾*N(SO₂CF₃)2^(1-)=[(Au(P(C₆H₅)3))2(C(CH₃)CHOC₂H₅)](N(SO₂CF₃)2)

There total 2 articles about (Au(P(C₆H₅)3))2(C(CH₃)CHOC₂H₅)⁽¹⁺⁾*N(SO₂CF₃)2^(1-)=[(Au(P(C₆H₅)3))2(C(CH₃)CHOC₂H₅)](N(SO₂CF₃)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

[bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold (I) (866395-16-6,1246810-76-3) + 2-((Z)-2-Ethoxy-1-methyl-vinyl)-benzo[1,3,2]dioxaborole → (triphenylphosphine)gold(I) chloride (14243-64-2) + [(Ph3P)2Au]+SbF6- (1259377-02-0) + (Au(P(C6H5)3))2(C(CH3)CHOC2H5)(1+)*N(SO2CF3)2(1-)=[(Au(P(C6H5)3))2(C(CH3)CHOC2H5)](N(SO2CF3)2) (1259488-31-7)

Guidance literature:

With Cs₂CO₃; In tetrahydrofuran; reaction at room temp.; flash chromy. (silica gel);

DOI:10.1002/anie.201003349

Reference yield:

[bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I) (866395-16-6,1246810-76-3) + 2-((Z)-2-Ethoxy-1-methyl-vinyl)-benzo[1,3,2]dioxaborole → (Au(P(C6H5)3))2(C(CH3)CHOC2H5)(1+)*N(SO2CF3)2(1-)=[(Au(P(C6H5)3))2(C(CH3)CHOC2H5)](N(SO2CF3)2) (1259488-31-7)

Guidance literature:

With caesium carbonate; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1002/chem.201503403

upstream raw materials:

[bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold (I)

[bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I)

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