4-hydroxyphenylpropionaldehyde

Base Information

• Chemical Name: 4-hydroxyphenylpropionaldehyde
• CAS No.: 90708-66-0
• Molecular Formula: C₉H₁₀O₂
• Molecular Weight: 150.177
• Mol file: 90708-66-0.mol

Synonyms:4-hydroxyphenylpropionaldehyde

Chemical Property of 4-hydroxyphenylpropionaldehyde

Chemical Property:

Purity/Quality:

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Technology Process of 4-hydroxyphenylpropionaldehyde

There total 5 articles about 4-hydroxyphenylpropionaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

[4-((4-(3-oxo-propyl)phenoxy)-diphenyl-methyl)phenoxy]-poly(styrene-co-divinylbenzene), copolymer 99:1, trityl loading: 1.47 mmol/g → 4-hydroxyphenylpropionaldehyde (90708-66-0)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1002/adsc.200303053

Reference yield: 95.0%

4-Propenyl-phenol (539-12-8) → 4-hydroxyphenylpropionaldehyde (90708-66-0)

Guidance literature:

With iodine; silver(l) oxide; In 1,4-dioxane; water; for 4h; Ambient temperature;

DOI:10.1246/cl.1984.341

Reference yield: 88.0%

carbon monoxide (201230-82-2) + 4-Vinylphenol (2628-17-3,24979-70-2) → dihydro-p-coumaryl aldehyde (20238-83-9) + 4-hydroxyphenylpropionaldehyde (90708-66-0)

Guidance literature:

With chloro(1,5-cyclooctadiene)rhodium(I) dimer; hydrogen; sodium 4-dodecylbenzenesulfonate; Sodium; 2-[bis-(2-diphenylphosphanyl-ethyl)-carbamoyl]-benzenesulfonate; In water; toluene; at 60 ℃; under 30003 Torr;

DOI:10.1016/j.cclet.2021.07.068

upstream raw materials:

4-Propenyl-phenol

carbon monoxide

4-Vinylphenol

3-(4-hydroxyphenyl)propan-1-ol