3,5-bis(3,5-bis[3-(tert-butyldimethylsilyloxy)propyloxy]benzyloxy)benzyl alcohol

Base Information

Chemical Name:3,5-bis(3,5-bis[3-(tert-butyldimethylsilyloxy)propyloxy]benzyloxy)benzyl alcohol
CAS No.:247123-01-9
Molecular Formula:C₅₇H₁₀₀O₁₁Si₄
Molecular Weight:1073.76
Hs Code.:

Synonyms:3,5-bis(3,5-bis[3-(tert-butyldimethylsilyloxy)propyloxy]benzyloxy)benzyl alcohol

Suppliers and Price of 3,5-bis(3,5-bis[3-(tert-butyldimethylsilyloxy)propyloxy]benzyloxy)benzyl alcohol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-bis(3,5-bis[3-(tert-butyldimethylsilyloxy)propyloxy]benzyloxy)benzyl alcohol

Chemical Property:

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Technology Process of 3,5-bis(3,5-bis[3-(tert-butyldimethylsilyloxy)propyloxy]benzyloxy)benzyl alcohol

There total 6 articles about 3,5-bis(3,5-bis[3-(tert-butyldimethylsilyloxy)propyloxy]benzyloxy)benzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 29654-55-5
5-(hydroxymethyl)benzene-1,3-diol

: 247122-96-9
3,5-bis[3-(tert-butyldimethylsilyloxy)propyloxy]benzyl bromide

: 247123-01-9
3,5-bis(3,5-bis[3-(tert-butyldimethylsilyloxy)propyloxy]benzyloxy)benzyl alcohol

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In acetone; for 24h;
DOI:10.1021/ol990836a

Reference yield:

: 89031-84-5
3-(tert-butyldimethylsilyloxy)propyl bromide

: 247123-01-9
3,5-bis(3,5-bis[3-(tert-butyldimethylsilyloxy)propyloxy]benzyloxy)benzyl alcohol

Guidance literature:: Multi-step reaction with 4 steps

1: 18-crown-6; K₂CO₃

2: 90 percent / Et₃N / CH₂Cl₂

3: 93 percent / LiBr / tetrahydrofuran

4: 91 percent / 18-crown-6; K₂CO₃ / acetone / 24 h

With 18-crown-6 ether; potassium carbonate; triethylamine; lithium bromide; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/ol990836a

Reference yield:

: 247122-94-7
3,5-bis[3-(tert-butyldimethylsilyloxy)propyloxy]benzyl alcohol

: 247123-01-9
3,5-bis(3,5-bis[3-(tert-butyldimethylsilyloxy)propyloxy]benzyloxy)benzyl alcohol

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / Et₃N / CH₂Cl₂

2: 93 percent / LiBr / tetrahydrofuran

3: 91 percent / 18-crown-6; K₂CO₃ / acetone / 24 h

With 18-crown-6 ether; potassium carbonate; triethylamine; lithium bromide; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/ol990836a