C₁₃H₁₇NO

Base Information

Chemical Name:C₁₃H₁₇NO
CAS No.:1609647-33-7
Molecular Formula:C₁₃H₁₇NO
Molecular Weight:203.284
Hs Code.:

Synonyms:C₁₃H₁₇NO

Suppliers and Price of C₁₃H₁₇NO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₇NO

Chemical Property:

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Technology Process of C₁₃H₁₇NO

There total 7 articles about C₁₃H₁₇NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1609647-31-5
C₂₀H₂₅NO₄S

: 1609647-33-7
C₁₃H₁₇NO

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 15h;
DOI:10.1055/s-0033-1340250

Reference yield:

: 1609647-12-2
3-ethylidene-1-(4-methylbenzyl)azetidine

: 1609647-33-7
C₁₃H₁₇NO

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 0.17 h / 20 °C

1.2: 15 h / Reflux

2.1: sodium hydride / tetrahydrofuran; mineral oil / 15 h / 20 °C

With sodium hydride; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1055/s-0033-1340250

Reference yield:

: 922-63-4
ethylacrolein

: 1609647-33-7
C₁₃H₁₇NO

Guidance literature:: Multi-step reaction with 7 steps

1.1: bromine / dichloromethane / 2.5 h / 0 - 20 °C

2.1: titanium tetrachloride; triethylamine / diethyl ether / 15 h / 0 - 20 °C

3.1: sodium tetrahydroborate / methanol / 20 °C

4.1: acetonitrile / 15 h / Reflux

5.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 120 °C / Microwave irradiation

6.1: dichloromethane / 0.17 h / 20 °C

6.2: 15 h / Reflux

7.1: sodium hydride / tetrahydrofuran; mineral oil / 15 h / 20 °C

With sodium tetrahydroborate; potassium tert-butylate; bromine; titanium tetrachloride; sodium hydride; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetonitrile; mineral oil;
DOI:10.1055/s-0033-1340250