5-[(1,3-Benzodioxol-5-ylmethyl)sulfonyl]-1-phenyl-1H-tetrazole

Base Information

Chemical Name:5-[(1,3-Benzodioxol-5-ylmethyl)sulfonyl]-1-phenyl-1H-tetrazole
CAS No.:1036244-18-4
Molecular Formula:C₁₅H₁₂N₄O₄S
Molecular Weight:344.351
Hs Code.:
DSSTox Substance ID:DTXSID701176952

Synonyms:DTXSID701176952;5-[(1,3-Benzodioxol-5-ylmethyl)sulfonyl]-1-phenyl-1H-tetrazole;1036244-18-4

Suppliers and Price of 5-[(1,3-Benzodioxol-5-ylmethyl)sulfonyl]-1-phenyl-1H-tetrazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-[(1,3-Benzodioxol-5-ylmethyl)sulfonyl]-1-phenyl-1H-tetrazole

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:4
Exact Mass:344.05792605
Heavy Atom Count:24
Complexity:534

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1OC2=C(O1)C=C(C=C2)CS(=O)(=O)C3=NN=NN3C4=CC=CC=C4

Technology Process of 5-[(1,3-Benzodioxol-5-ylmethyl)sulfonyl]-1-phenyl-1H-tetrazole

There total 6 articles about 5-[(1,3-Benzodioxol-5-ylmethyl)sulfonyl]-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 425652-61-5
5-((benzo[d][1,3]dioxol-5-ylmethyl)thio)-1-phenyl-1H-tetrazole

: 1036244-18-4
5-((benzo[d][1,3]dioxol-5-ylmethyl)sulfonyl)-1-phenyl-1H-tetrazole

Guidance literature:: With ammonium molybdate; dihydrogen peroxide; In ethanol; at 0 - 20 ℃; for 8h;
DOI:10.1002/cmdc.201900390

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 1036244-18-4
5-((benzo[d][1,3]dioxol-5-ylmethyl)sulfonyl)-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / 0.25 h / 0 °C / Inert atmosphere

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

3: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol / 7 h / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; hexaammonium heptamolybdate tetrahydrate; di-isopropyl azodicarboxylate; dihydrogen peroxide; triphenylphosphine; In tetrahydrofuran; methanol; ethanol; 2: Mitsunobu type reaction;
DOI:10.1080/10286020.2010.546356

Reference yield:

: 495-76-1
piperonol

: 1036244-18-4
5-((benzo[d][1,3]dioxol-5-ylmethyl)sulfonyl)-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 2 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

2: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol / 7 h / 0 - 20 °C / Inert atmosphere

With hexaammonium heptamolybdate tetrahydrate; di-isopropyl azodicarboxylate; dihydrogen peroxide; triphenylphosphine; In tetrahydrofuran; ethanol; 1: Mitsunobu type reaction;
DOI:10.1080/10286020.2010.546356