(αS,5S)-α-<(benzyloxycarbonyl)amino>-5-isoxazolidineacetic acid methylidene ester

Base Information

Chemical Name:(αS,5S)-α-<(benzyloxycarbonyl)amino>-5-isoxazolidineacetic acid methylidene ester
CAS No.:105834-76-2
Molecular Formula:C₁₄H₁₆N₂O₅
Molecular Weight:292.291
Hs Code.:

Synonyms:(αS,5S)-α-<(benzyloxycarbonyl)amino>-5-isoxazolidineacetic acid methylidene ester

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Chemical Property of (αS,5S)-α-<(benzyloxycarbonyl)amino>-5-isoxazolidineacetic acid methylidene ester

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Technology Process of (αS,5S)-α-<(benzyloxycarbonyl)amino>-5-isoxazolidineacetic acid methylidene ester

There total 5 articles about (αS,5S)-α-<(benzyloxycarbonyl)amino>-5-isoxazolidineacetic acid methylidene ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 105834-71-7,105928-18-5
(αS,5S)-2-(2',3'-O-isopropylidene-5'-O-trityl-α-D-ribofuranosyl)-α-<(benzyloxycarbonyl)amino>-5-isoxazolidine-acetic acid methylidene ester

: 105834-76-2
(αS,5S)-α-<(benzyloxycarbonyl)amino>-5-isoxazolidineacetic acid methylidene ester

Guidance literature:: With formic acid; Ambient temperature;
DOI:10.1021/jo00252a035

Reference yield:

: 90292-75-4
(S)-3-Benzyloxycarbonyl-5-oxo-4-vinyltetrahydro-1,3-oxazole

: 105834-76-2
(αS,5S)-α-<(benzyloxycarbonyl)amino>-5-isoxazolidineacetic acid methylidene ester

Guidance literature:: Multi-step reaction with 2 steps

1: CHCl₃ / 36 h / Heating

2: 98percent formic acid / Ambient temperature

With formic acid; In chloroform;
DOI:10.1021/jo00252a035

Reference yield:

: 115481-99-7
(S)-3-benzyloxycarbonyl-4-(2-methylthioethyl)oxazolidin-5-one

: 105834-76-2
(αS,5S)-α-<(benzyloxycarbonyl)amino>-5-isoxazolidineacetic acid methylidene ester

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / sodium metaperiodate / methanol; H₂O / 5 h

2: 65 percent / triethyl phosphite / xylene / 48 h / Heating

3: CHCl₃ / 36 h / Heating

4: 98percent formic acid / Ambient temperature

With sodium periodate; formic acid; triethyl phosphite; In methanol; chloroform; water; xylene;
DOI:10.1021/jo00252a035