(2S,3S,4S)-5-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethyl-pentanal

Base Information

Chemical Name:(2S,3S,4S)-5-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethyl-pentanal
CAS No.:85828-12-2
Molecular Formula:C₂₀H₃₄O₃Si
Molecular Weight:350.574
Hs Code.:

Synonyms:(2S,3S,4S)-5-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethyl-pentanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S,4S)-5-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethyl-pentanal

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Technology Process of (2S,3S,4S)-5-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethyl-pentanal

There total 6 articles about (2S,3S,4S)-5-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethyl-pentanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: (3S,4R,5R)-6-Benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-2-hydroxy-3,5-dimethyl-hexanenitrile

: 85828-12-2
(2S,3S,4S)-5-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethyl-pentanal

Guidance literature:: With sodium hydroxide; In diethyl ether; at 22 ℃; for 2h;
DOI:10.1016/S0040-4039(00)98954-8

Reference yield:

: 73814-78-5,85880-73-5
(2R,3S,4S)-1-Benzyloxy-2,4-dimethyl-hex-5-en-3-ol

: 85828-12-2
(2S,3S,4S)-5-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethyl-pentanal

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / imidazole / dimethylformamide / 120 h

2: 1.) O₃, 2.) Zn, 50percent aq. acetic acid / 1.) CH₂Cl₂, -78 deg C, 2.) ether, 2 h

With 1H-imidazole; ozone; acetic acid; zinc; In N,N-dimethyl-formamide;
DOI:10.1021/ja00023a029

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 85828-12-2
(2S,3S,4S)-5-Benzyloxy-3-(tert-butyl-dimethyl-silanyloxy)-2,4-dimethyl-pentanal

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / imidazole / dimethylformamide / 120 h

2: 1.) O₃, 2.) Zn, 50percent aq. acetic acid / 1.) CH₂Cl₂, -78 deg C, 2.) ether, 2 h

With 1H-imidazole; ozone; acetic acid; zinc; In N,N-dimethyl-formamide;
DOI:10.1021/ja00023a029